methyl (tert-butyl 3,4-di-O-benzyl-α-L-idopyranosyluronate)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(tert-butyl 3-O-benzyl-α-L-idopyranosideuronate)

Base Information

• Chemical Name: methyl (tert-butyl 3,4-di-O-benzyl-α-L-idopyranosyluronate)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(tert-butyl 3-O-benzyl-α-L-idopyranosideuronate)
• CAS No.: 1075217-50-3
• Molecular Formula: C₅₅H₆₉N₃O₁₇
• Molecular Weight: 1044.16

Synonyms:methyl (tert-butyl 3,4-di-O-benzyl-α-L-idopyranosyluronate)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(tert-butyl 3-O-benzyl-α-L-idopyranosideuronate)

Chemical Property of methyl (tert-butyl 3,4-di-O-benzyl-α-L-idopyranosyluronate)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(tert-butyl 3-O-benzyl-α-L-idopyranosideuronate)

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Technology Process of methyl (tert-butyl 3,4-di-O-benzyl-α-L-idopyranosyluronate)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(tert-butyl 3-O-benzyl-α-L-idopyranosideuronate)

There total 1 articles about methyl (tert-butyl 3,4-di-O-benzyl-α-L-idopyranosyluronate)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(tert-butyl 3-O-benzyl-α-L-idopyranosideuronate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

methyl (tert-butyl 3,4-di-O-benzyl-α-L-idopyranosyluronate)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-6-O-(4-methoxyphenyl)-α-D-glucopyranosyl]-(1->4)-(tert-butyl 3-O-benzyl-α-L-idopyranosideuronate) (1075217-48-9) → methyl (tert-butyl 3,4-di-O-benzyl-α-L-idopyranosyluronate)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(tert-butyl 3-O-benzyl-α-L-idopyranosideuronate) (1075217-50-3)

Guidance literature:

With ammonium cerium (IV) nitrate; In water; acetonitrile; at 20 ℃; for 1h;

DOI:10.1016/j.tet.2008.08.021

Reference yield: 98.0%

methyl (tert-butyl 3,4-di-O-benzyl-α-L-idopyranosyluronate)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(tert-butyl 3-O-benzyl-α-L-idopyranosideuronate) (1075217-50-3) → methyl (3,4-di-O-benzyl-α-L-idopyranosyluronic acid)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(3-O-benzyl-α-L-idopyranosideuronic acid) (1075217-52-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 1h;

DOI:10.1016/j.tet.2008.08.021

upstream raw materials:

methyl (tert-butyl 3,4-di-O-benzyl-α-L-idopyranosyluronate)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-6-O-(4-methoxyphenyl)-α-D-glucopyranosyl]-(1->4)-(tert-butyl 3-O-benzyl-α-L-idopyranosideuronate)

Downstream raw materials:

methyl (3,4-di-O-benzyl-α-L-idopyranosyluronic acid)-(1->4)-[2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl]-(1->4)-(3-O-benzyl-α-L-idopyranosideuronic acid)

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