3,5-Bis-((E)-2-{3,5-bis-[(E)-2-(4-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-benzaldehyde

Base Information

• Chemical Name: 3,5-Bis-((E)-2-{3,5-bis-[(E)-2-(4-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-benzaldehyde
• CAS No.: 363622-84-8
• Molecular Formula: C₁₀₃H₁₃₈O₅
• Molecular Weight: 1456.23

Synonyms:3,5-Bis-((E)-2-{3,5-bis-[(E)-2-(4-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-benzaldehyde

Chemical Property of 3,5-Bis-((E)-2-{3,5-bis-[(E)-2-(4-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-benzaldehyde

Chemical Property:

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Technology Process of 3,5-Bis-((E)-2-{3,5-bis-[(E)-2-(4-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-benzaldehyde

There total 1 articles about 3,5-Bis-((E)-2-{3,5-bis-[(E)-2-(4-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

[3,5-Bis-((E)-2-{3,5-bis-[(E)-2-(4-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-methanol → 3,5-Bis-((E)-2-{3,5-bis-[(E)-2-(4-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-benzaldehyde (363622-84-8)

Guidance literature:

With manganese(IV) oxide; In dichloromethane; at 20 ℃;

DOI:10.1021/jo015764r

Reference yield: 66.0%

3,5-Bis-((E)-2-{3,5-bis-[(E)-2-(4-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-benzaldehyde (363622-84-8) + {3,5-Bis-[(E)-2-(4-cyano-phenyl)-vinyl]-benzyl}-phosphonic acid diethyl ester (363622-70-2) → C128H154N2O4

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 4.5h;

DOI:10.1021/jo015764r

Reference yield:

1-acetyloxymethyl-3,5-bis(diethoxyphosphorylmethyl)benzene (363622-49-5) + 3,5-Bis-((E)-2-{3,5-bis-[(E)-2-(4-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-benzaldehyde (363622-84-8) → 3,5-Bis-((E)-2-{3,5-bis-[(E)-2-(4-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-benzoic acid + C127H108O9(C11H22)8

Guidance literature:

1-acetyloxymethyl-3,5-bis(diethoxyphosphorylmethyl)benzene; 3,5-Bis-((E)-2-{3,5-bis-[(E)-2-(4-dodecyloxy-phenyl)-vinyl]-phenyl}-vinyl)-benzaldehyde; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 24h;

With sodium hydroxide; at 20 ℃; for 2h; Further stages. Title compound not separated from byproducts.;

DOI:10.1021/jo015764r

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