trans-5-phenyl-4-pentenamide

Base Information

Chemical Name:trans-5-phenyl-4-pentenamide
CAS No.:30154-22-4
Molecular Formula:C₁₁H₁₃NO
Molecular Weight:175.23
Hs Code.:

Synonyms:trans-5-phenyl-4-pentenamide

Suppliers and Price of trans-5-phenyl-4-pentenamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trans-5-phenyl-4-pentenamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trans-5-phenyl-4-pentenamide

There total 7 articles about trans-5-phenyl-4-pentenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 22768-07-6,121746-04-1,93845-04-6
(E)-ethyl 5-phenylpent-4-enoate

: 30154-22-4
trans-5-phenyl-4-pentenamide

Guidance literature:: With trimethylaluminum; ammonium chloride; In toluene; at 55 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1021/ja5046296

Reference yield:

: 28525-69-1
(4E)-5-phenyl-4-pentenoic acid

: 30154-22-4
trans-5-phenyl-4-pentenamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 1.5 h / Heating

2: ammonium hydroxide, K₂CO₃ / benzene; diethyl ether / Ambient temperature

With ammonium hydroxide; thionyl chloride; potassium carbonate; In diethyl ether; benzene;
DOI:10.1021/ja00009a041

Reference yield:

: 21087-29-6
trans-3-phenylprop-2-enyl chloride

: 30154-22-4
trans-5-phenyl-4-pentenamide

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent

2: 75 percent / NaCl / dimethylsulfoxide; H₂O / 6 h / Heating

3: 10percent KOH / methanol; H₂O / 2 h / Heating

4: thionyl chloride / 1.5 h / Heating

5: ammonium hydroxide, K₂CO₃ / benzene; diethyl ether / Ambient temperature

With potassium hydroxide; ammonium hydroxide; thionyl chloride; potassium carbonate; sodium chloride; In methanol; diethyl ether; water; dimethyl sulfoxide; benzene;
DOI:10.1021/ja00009a041