cis-2,3,4,4a,5,6,7,11c-octahydro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole

Base Information

Chemical Name:cis-2,3,4,4a,5,6,7,11c-octahydro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole
CAS No.:85923-46-2
Molecular Formula:C₂₂H₂₄N₂O₃S
Molecular Weight:396.51
Hs Code.:

Synonyms:cis-2,3,4,4a,5,6,7,11c-octahydro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole

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Chemical Property of cis-2,3,4,4a,5,6,7,11c-octahydro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole

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Technology Process of cis-2,3,4,4a,5,6,7,11c-octahydro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole

There total 5 articles about cis-2,3,4,4a,5,6,7,11c-octahydro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 85923-43-9
2-chloroethyl cis-2,3,4,4a,5,6,7,11c-octahydro-7<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole-1-carboxylate

: 85923-46-2
cis-2,3,4,4a,5,6,7,11c-octahydro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole

Guidance literature:: With samarium diiodide; In tetrahydrofuran; for 7h; Heating;
DOI:10.1021/ja00352a037

Reference yield:

: 5416-80-8
2-methyl-1H-indole-3-carbaldehyde

: 85923-46-2
cis-2,3,4,4a,5,6,7,11c-octahydro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) sodium hydride, 2.) imidazole / 1.) glyme, 20 deg C, 1.5 h, reflux, 15 min, 2.) 20 deg C, 15 h

2: 2.) Na₂SO₄ / 1.) benzene, 1 h, 2.) 2 h

3: 79 percent / diisopropylethylamine / chlorobenzene / 1.25 h / 135 °C

4: 86 percent / zinc, acetic acid / H₂O / 15 h / 20 °C

With 1H-imidazole; sodium hydride; acetic acid; sodium sulfate; N-ethyl-N,N-diisopropylamine; zinc; In water; chlorobenzene;
DOI:10.1021/ja00352a037

Reference yield:

: 85923-42-8
N-<<(4-methoxybenzenesulfonyl)-2-methyl-1H-indol-3-yl>methylene>-4-pentenylamine

: 85923-46-2
cis-2,3,4,4a,5,6,7,11c-octahydro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / diisopropylethylamine / chlorobenzene / 1.25 h / 135 °C

2: 86 percent / zinc, acetic acid / H₂O / 15 h / 20 °C

With acetic acid; N-ethyl-N,N-diisopropylamine; zinc; In water; chlorobenzene;
DOI:10.1021/ja00352a037