C₄₅H₅₈N₈O₆Si

Base Information

Chemical Name:C₄₅H₅₈N₈O₆Si
CAS No.:1428135-48-1
Molecular Formula:C₄₅H₅₈N₈O₆Si
Molecular Weight:835.091
Hs Code.:

C<sub>45</sub>H<sub>58</sub>N<sub>8</sub>O<sub>6</sub>Si

Synonyms:C₄₅H₅₈N₈O₆Si

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Chemical Property of C₄₅H₅₈N₈O₆Si

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Technology Process of C₄₅H₅₈N₈O₆Si

There total 7 articles about C₄₅H₅₈N₈O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.3%

: C₂₉H₃₂N₆Si*4ClH

: 74761-39-0
(2S,3S)-2-((methoxycarbonyl)amino)-3-methylpentanoic acid

: 1428135-48-1
C₄₅H₅₈N₈O₆Si

Guidance literature:: C₂₉H₃₂N₆Si*4ClH; (2S,3S)-2-((methoxycarbonyl)amino)-3-methylpentanoic acid; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; acetonitrile; at 20 ℃; for 0.166667h;

With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; In tetrahydrofuran; ethyl acetate; acetonitrile; for 3h;

Reference yield:

: 1428136-85-9
C₃₉H₄₈N₆O₄Si

: 1428135-48-1
C₄₅H₅₈N₈O₆Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

1.2: 0.5 h

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran; acetonitrile / 0.17 h / 20 °C

2.2: 3 h

With N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; acetonitrile;

Reference yield:

: 268224-19-7
(2R,5R)-2-(((iodomethyl)dimethylsilyl)methyl)-5-isopropyl-3,6-dimethoxy-2,5-dihydropyrazine

: 1428135-48-1
C₄₅H₅₈N₈O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogenchloride; water / methanol / 5 h / 20 °C

1.2: 7 h / 20 °C

1.3: 15 h / 20 °C

2.1: water; potassium hydroxide / methanol / 15 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine; HATU / 6.5 h / 0 °C

4.1: acetic acid / 5 h / 60 °C

5.1: potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 16 h / 80 °C

6.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

6.2: 0.5 h

7.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran; acetonitrile / 0.17 h / 20 °C

7.2: 3 h

With hydrogenchloride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; water; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; acetonitrile;