[3,7,11-trimethyl-dodecyl-2,4,6,10-tetraenyl]-triphenylphosphonium chloride

Base Information

Chemical Name:[3,7,11-trimethyl-dodecyl-2,4,6,10-tetraenyl]-triphenylphosphonium chloride
CAS No.:131801-83-7
Molecular Formula:C₃₃H₃₈P*Cl
Molecular Weight:501.091
Hs Code.:

Synonyms:[3,7,11-trimethyl-dodecyl-2,4,6,10-tetraenyl]-triphenylphosphonium chloride

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Chemical Property of [3,7,11-trimethyl-dodecyl-2,4,6,10-tetraenyl]-triphenylphosphonium chloride

Chemical Property:

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Technology Process of [3,7,11-trimethyl-dodecyl-2,4,6,10-tetraenyl]-triphenylphosphonium chloride

There total 4 articles about [3,7,11-trimethyl-dodecyl-2,4,6,10-tetraenyl]-triphenylphosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124160-98-1
3,7,11-trimethyldodeca-2,4,6,10-tetraen-1-yl-triphenylphosphonium chloride

: 131801-83-7
[3,7,11-trimethyl-dodecyl-2,4,6,10-tetraenyl]-triphenylphosphonium chloride

: 131801-85-9
(2E,4E,6Z)-3,7,11-trimethyldodeca-2,4,6,10-tetraen-1-yl-triphenylphosphonium chloride

Guidance literature:: With potassium carbonate; In ethyl acetate; acetone; at 30 - 50 ℃; for 18h; Temperature; Overall yield = 48.5 g;

Reference yield:

: 145571-82-0
(all-E)-3,7,11-Trimethyldodeca-4,6,10-trien-1-yn-3-ol

: 131801-83-7
[3,7,11-trimethyl-dodecyl-2,4,6,10-tetraenyl]-triphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / H₂, 2,2'-(ethylenedithio)bis(ethanol), Et₃N / Lindlar catalyst / CH₂Cl₂ / 750.06 Torr / Ambient temperature

2: 1) AcOH, 2) 2percent aq. NaCl / 1) hexane, 60 deg C, 2.5 h, 2) CH₂Cl₂

With 2,2'-ethane-1,2-diylbissulfanyl-bis-ethanol; hydrogen; acetic acid; triethylamine; sodium chloride; Lindlar's catalyst; In dichloromethane;
DOI:10.1002/hlca.19920750611

Reference yield:

: 141-10-6,3548-78-5
pseudoionone

: 131801-83-7
[3,7,11-trimethyl-dodecyl-2,4,6,10-tetraenyl]-triphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Li, liq. NH₃ / 2) THF, 10 deg C, 5 min

2: 92 percent / H₂, 2,2'-(ethylenedithio)bis(ethanol), Et₃N / Lindlar catalyst / CH₂Cl₂ / 750.06 Torr / Ambient temperature

3: 1) AcOH, 2) 2percent aq. NaCl / 1) hexane, 60 deg C, 2.5 h, 2) CH₂Cl₂

With 2,2'-ethane-1,2-diylbissulfanyl-bis-ethanol; ammonia; hydrogen; lithium; acetic acid; triethylamine; sodium chloride; Lindlar's catalyst; In dichloromethane;
DOI:10.1002/hlca.19920750611