hexaazaoctadecahydrocoronenium perfluoro-7,7,8,8-tetracyano-p-benzoquinonedimethanediide

Base Information

• Chemical Name: hexaazaoctadecahydrocoronenium perfluoro-7,7,8,8-tetracyano-p-benzoquinonedimethanediide
• CAS No.: 123265-19-0
• Molecular Formula: C₁₂F₄N₄*C₁₈H₂₄N₆
• Molecular Weight: 600.581
• Mol file: 123265-19-0.mol

Synonyms:hexaazaoctadecahydrocoronenium perfluoro-7,7,8,8-tetracyano-p-benzoquinonedimethanediide

Chemical Property of hexaazaoctadecahydrocoronenium perfluoro-7,7,8,8-tetracyano-p-benzoquinonedimethanediide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of hexaazaoctadecahydrocoronenium perfluoro-7,7,8,8-tetracyano-p-benzoquinonedimethanediide

There total 2 articles about hexaazaoctadecahydrocoronenium perfluoro-7,7,8,8-tetracyano-p-benzoquinonedimethanediide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2a,4a,6a,8a,10a,12a-hexaazacoronene-1,3,5,7,9,11(2H,4H,6H,8H,10H,12H)-hexone (92187-33-2) → hexaazaoctadecahydrocoronenium perfluoro-7,7,8,8-tetracyano-p-benzoquinonedimethanediide (123265-19-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / Borane / tetrahydrofuran / 16 h / Heating

2: AgNO₃ / CH₂Cl₂; acetonitrile

With borane; silver nitrate; In tetrahydrofuran; dichloromethane; acetonitrile;

DOI:10.1021/ja00157a058

Reference yield:

2,3,5,6-tetrafluoro-7,7',8,8'-tetracyanoquinodimethane (29261-33-4) + hexaazaoctadecahydrocoronene (92187-27-4) → hexaazaoctadecahydrocoronenium perfluoro-7,7,8,8-tetracyano-p-benzoquinonedimethanediide (123265-19-0)

Guidance literature:

With silver nitrate; In dichloromethane; acetonitrile;

DOI:10.1021/ja00157a058

upstream raw materials:

2,3,5,6-tetrafluoro-7,7',8,8'-tetracyanoquinodimethane

hexaazaoctadecahydrocoronene

2a,4a,6a,8a,10a,12a-hexaazacoronene-1,3,5,7,9,11(2H,4H,6H,8H,10H,12H)-hexone

Refernces