4-butyl-5-(4-(2,4-dichlorobenzyloxy)phenyl)-2H-1,2,4-triazole-3(4H)-one

Base Information

Chemical Name:4-butyl-5-(4-(2,4-dichlorobenzyloxy)phenyl)-2H-1,2,4-triazole-3(4H)-one
CAS No.:1630013-20-5
Molecular Formula:C₁₉H₁₉Cl₂N₃O₂
Molecular Weight:392.285
Hs Code.:

Synonyms:4-butyl-5-(4-(2,4-dichlorobenzyloxy)phenyl)-2H-1,2,4-triazole-3(4H)-one

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Chemical Property of 4-butyl-5-(4-(2,4-dichlorobenzyloxy)phenyl)-2H-1,2,4-triazole-3(4H)-one

Chemical Property:

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Technology Process of 4-butyl-5-(4-(2,4-dichlorobenzyloxy)phenyl)-2H-1,2,4-triazole-3(4H)-one

There total 6 articles about 4-butyl-5-(4-(2,4-dichlorobenzyloxy)phenyl)-2H-1,2,4-triazole-3(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.6%

: 1630012-73-5
C₁₉H₂₁Cl₂N₃O₃

: 1630013-20-5
4-butyl-5-(4-(2,4-dichlorobenzyloxy)phenyl)-2H-1,2,4-triazole-3(4H)-one

Guidance literature:: With potassium hydroxide; In water; at 100 ℃; for 48h;
DOI:10.2174/1570180810666131122003939

Reference yield:

: 56441-85-1
4-(2,4-Dichlorbenzyloxy)-benzoesaeureaethylester

: 1630013-20-5
4-butyl-5-(4-(2,4-dichlorobenzyloxy)phenyl)-2H-1,2,4-triazole-3(4H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazine hydrate / ethanol / 6 h / Reflux

2: dichloromethane / 6 h / 50 °C

3: ethanol / 4 h / 80 °C

4: potassium hydroxide / water / 48 h / 100 °C

With hydrazine hydrate; potassium hydroxide; In ethanol; dichloromethane; water;
DOI:10.2174/1570180810666131122003939

Reference yield:

: 120-47-8
Ethyl 4-hydroxybenzoate

: 1630013-20-5
4-butyl-5-(4-(2,4-dichlorobenzyloxy)phenyl)-2H-1,2,4-triazole-3(4H)-one

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / acetonitrile / 0.5 h / Reflux

1.2: 3 h / Reflux

2.1: hydrazine hydrate / ethanol / 6 h / Reflux

3.1: dichloromethane / 6 h / 50 °C

4.1: ethanol / 4 h / 80 °C

5.1: potassium hydroxide / water / 48 h / 100 °C

With hydrazine hydrate; potassium hydroxide; In ethanol; dichloromethane; water; acetonitrile;
DOI:10.2174/1570180810666131122003939