methyl (+/-)--<1-<1-<(methoxycarbonyl)amino>ethyl>-2-butenyl>-N-phenylthiocarbamate

Base Information

• Chemical Name: methyl (+/-)--<1-<1-<(methoxycarbonyl)amino>ethyl>-2-butenyl>-N-phenylthiocarbamate
• CAS No.: 93062-01-2
• Molecular Formula: C₁₆H₂₂N₂O₄S
• Molecular Weight: 338.428

Synonyms:methyl (+/-)--<1-<1-<(methoxycarbonyl)amino>ethyl>-2-butenyl>-N-phenylthiocarbamate

Chemical Property of methyl (+/-)--<1-<1-<(methoxycarbonyl)amino>ethyl>-2-butenyl>-N-phenylthiocarbamate

Chemical Property:

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Technology Process of methyl (+/-)--<1-<1-<(methoxycarbonyl)amino>ethyl>-2-butenyl>-N-phenylthiocarbamate

There total 4 articles about methyl (+/-)--<1-<1-<(methoxycarbonyl)amino>ethyl>-2-butenyl>-N-phenylthiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

phenylmagnesium bromide + (3R,6S)-1-[(E)-Methoxycarbonylimino]-3,6-dimethyl-3,6-dihydro-1H-1λ4-[1,2]thiazine-2-carboxylic acid methyl ester (93133-35-8) → methyl (+/-)--<1-<1-<(methoxycarbonyl)amino>ethyl>-2-butenyl>-N-phenylthiocarbamate (93062-01-2)

Guidance literature:

In tetrahydrofuran; diethyl ether; at -60 ℃; for 0.333333h;

DOI:10.1021/ja00337a037

Reference yield:

phenylmagnesium bromide + (3R,6R)-1-[(E)-Methoxycarbonylimino]-3,6-dimethyl-3,6-dihydro-1H-1λ4-[1,2]thiazine-2-carboxylic acid methyl ester (93133-38-1) → methyl (+/-)--<1-<1-<(methoxycarbonyl)amino>ethyl>-2-butenyl>-N-phenylthiocarbamate (93062-01-2)

Guidance literature:

In tetrahydrofuran; diethyl ether; at -60 ℃; for 0.333333h;

DOI:10.1021/ja00337a037

Reference yield:

(2E,4E)-hexa-2,4-diene (5194-51-4) → methyl (+/-)--<1-<1-<(methoxycarbonyl)amino>ethyl>-2-butenyl>-N-phenylthiocarbamate (93062-01-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 71 percent / benzene / 17 h / Ambient temperature

2: 92 percent / diethyl ether; tetrahydrofuran / 0.33 h / -60 °C

In tetrahydrofuran; diethyl ether; benzene;

DOI:10.1021/ja00337a037

upstream raw materials:

(3R,6S)-1-[(E)-Methoxycarbonylimino]-3,6-dimethyl-3,6-dihydro-1H-1λ⁴-[1,2]thiazine-2-carboxylic acid methyl ester

(3R,6R)-1-[(E)-Methoxycarbonylimino]-3,6-dimethyl-3,6-dihydro-1H-1λ⁴-[1,2]thiazine-2-carboxylic acid methyl ester

(2E,4E)-hexa-2,4-diene

(E,Z)-2,4-hexadiene

Downstream raw materials:

(+/-)--4,5-bis<<(4-methylphenyl)sulfonyl>amino>-2-hexene

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