3-Phenyl-5-methyl-4-isoxazolylhydrazine

Base Information

Chemical Name:3-Phenyl-5-methyl-4-isoxazolylhydrazine
CAS No.:76270-19-4
Molecular Formula:C₁₀H₁₁N₃O
Molecular Weight:189.217
Hs Code.:

Synonyms:3-Phenyl-5-methyl-4-isoxazolylhydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Phenyl-5-methyl-4-isoxazolylhydrazine

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Technology Process of 3-Phenyl-5-methyl-4-isoxazolylhydrazine

There total 2 articles about 3-Phenyl-5-methyl-4-isoxazolylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-Methyl-3-phenyl-isoxazole-4-diazonium; chloride

: 76270-19-4
3-Phenyl-5-methyl-4-isoxazolylhydrazine

Guidance literature:: With tin chloride; In hydrogenchloride; at 0 ℃; for 1h; Yield given;
DOI:10.1007/BF01156379

Reference yield:

: 21169-65-3
5-methyl-3-phenyl-1,2-oxazole-4-amine

: 76270-19-4
3-Phenyl-5-methyl-4-isoxazolylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: nitrosylsulfuric acid / acetic acid / 0.5 h

2: tin chloride / HCl / 1 h / 0 °C

With nitrosylsulfuric acid; tin chloride; In hydrogenchloride; acetic acid;
DOI:10.1007/BF01156379