(2R,3R)-1,1-bis-[N-((1'S)-1'-phenyl-2'-hydroxyethyl)aminocarbonyl]-2,3-diphenylcyclopropane

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Chemical Name:(2R,3R)-1,1-bis-[N-((1'S)-1'-phenyl-2'-hydroxyethyl)aminocarbonyl]-2,3-diphenylcyclopropane
CAS No.:1256379-78-8
Molecular Formula:C₃₃H₃₂N₂O₄
Molecular Weight:520.628
Hs Code.:

Synonyms:(2R,3R)-1,1-bis-[N-((1'S)-1'-phenyl-2'-hydroxyethyl)aminocarbonyl]-2,3-diphenylcyclopropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-1,1-bis-[N-((1'S)-1'-phenyl-2'-hydroxyethyl)aminocarbonyl]-2,3-diphenylcyclopropane

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Technology Process of (2R,3R)-1,1-bis-[N-((1'S)-1'-phenyl-2'-hydroxyethyl)aminocarbonyl]-2,3-diphenylcyclopropane

There total 1 articles about (2R,3R)-1,1-bis-[N-((1'S)-1'-phenyl-2'-hydroxyethyl)aminocarbonyl]-2,3-diphenylcyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1256379-72-2
C₁₇H₁₄O₄

: 20989-17-7
(2S)-2-phenylglycinol

: 1256379-78-8
(2R,3R)-1,1-bis-[N-((1'S)-1'-phenyl-2'-hydroxyethyl)aminocarbonyl]-2,3-diphenylcyclopropane

Guidance literature:: C₁₇H₁₄O₄; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

(2S)-2-phenylglycinol; With triethylamine; In dichloromethane; at 0 - 20 ℃; for 1.66667h; Inert atmosphere;
DOI:10.1016/j.tetasy.2010.07.021

Reference yield: 73.0%

: 1256379-78-8
(2R,3R)-1,1-bis-[N-((1'S)-1'-phenyl-2'-hydroxyethyl)aminocarbonyl]-2,3-diphenylcyclopropane

: 1256379-70-0
(2R,3R)-1,1-di[(4'S)-4'-phenyloxazolin-2'-yl]-2,3-diphenylcyclopropane

Guidance literature:: (2R,3R)-1,1-bis-[N-((1'S)-1'-phenyl-2'-hydroxyethyl)aminocarbonyl]-2,3-diphenylcyclopropane; With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

With sodium hydroxide; In methanol; water; at 20 ℃; for 2h;
DOI:10.1016/j.tetasy.2010.07.021