(R)-N-(tert-butyl)oxycarbonyl-N-methyl-3-((3'-propanol)phenoxy)-3-phenylpropanamine

Base Information

Chemical Name:(R)-N-(tert-butyl)oxycarbonyl-N-methyl-3-((3'-propanol)phenoxy)-3-phenylpropanamine
CAS No.:1241411-21-1
Molecular Formula:C₂₄H₃₃NO₄
Molecular Weight:399.53
Hs Code.:

Synonyms:(R)-N-(tert-butyl)oxycarbonyl-N-methyl-3-((3'-propanol)phenoxy)-3-phenylpropanamine

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Chemical Property of (R)-N-(tert-butyl)oxycarbonyl-N-methyl-3-((3'-propanol)phenoxy)-3-phenylpropanamine

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Technology Process of (R)-N-(tert-butyl)oxycarbonyl-N-methyl-3-((3'-propanol)phenoxy)-3-phenylpropanamine

There total 2 articles about (R)-N-(tert-butyl)oxycarbonyl-N-methyl-3-((3'-propanol)phenoxy)-3-phenylpropanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1241411-20-0
(R)-N-(tert-butyl)oxycarbonyl-N-methyl-3-((2'-allyl)phenoxy)-3-phenylpropanamine

: 1241411-21-1
(R)-N-(tert-butyl)oxycarbonyl-N-methyl-3-((3'-propanol)phenoxy)-3-phenylpropanamine

Guidance literature:: (R)-N-(tert-butyl)oxycarbonyl-N-methyl-3-((2'-allyl)phenoxy)-3-phenylpropanamine; With borane-THF; In tetrahydrofuran; at 0 - 22 ℃; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 0 - 22 ℃; for 12h;
DOI:10.1002/jlcr.1744

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1241411-21-1
(R)-N-(tert-butyl)oxycarbonyl-N-methyl-3-((3'-propanol)phenoxy)-3-phenylpropanamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 0 - 20 °C

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 22 °C / Inert atmosphere

3.1: borane-THF / tetrahydrofuran / 0 - 22 °C / Inert atmosphere

3.2: 12 h / 0 - 22 °C

With borane-THF; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; 2.1: Mitsunobu reaction;
DOI:10.1002/jlcr.1744