Technology Process of C33H37N3O4
There total 6 articles about C33H37N3O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
dimethyl sulfoxide;
at 25 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/ol301331t
- Guidance literature:
-
Multi-step reaction with 2 steps
1: water; toluene-4-sulfonic acid / acetone / 24 h / 70 °C
2: potassium hydroxide / dimethyl sulfoxide / 2 h / 25 °C / Inert atmosphere
With
water; toluene-4-sulfonic acid; potassium hydroxide;
In
dimethyl sulfoxide; acetone;
DOI:10.1021/ol301331t
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 - 20 °C / Cooling with ice
2.1: 2,6-dimethylpyridine; t-butyldimethylsiyl triflate / dichloromethane / 1 h / 0 °C
2.2: 0 °C
3.1: imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate / methanol / 24 h / 0 °C
4.1: water; toluene-4-sulfonic acid / acetone / 24 h / 70 °C
5.1: potassium hydroxide / dimethyl sulfoxide / 2 h / 25 °C / Inert atmosphere
With
2,6-dimethylpyridine; imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; t-butyldimethylsiyl triflate; water; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; potassium hydroxide;
In
methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; mineral oil;
DOI:10.1021/ol301331t
