Technology Process of (4R,7R)-4-Benzyloxy-7-(tert-butyl-dimethyl-silanyloxy)-decanedial
There total 4 articles about (4R,7R)-4-Benzyloxy-7-(tert-butyl-dimethyl-silanyloxy)-decanedial which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium periodate; osmium(VIII) oxide; potassium hydrogencarbonate;
In
acetonitrile;
Ambient temperature;
DOI:10.1016/0040-4039(94)88291-6
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 87 percent / CuI / tetrahydrofuran / -40 °C
2: 86 percent / NaH, Bu4NBr / tetrahydrofuran / Ambient temperature
3: 100 percent / imidazole / dimethylformamide / Ambient temperature
4: 85 percent / OsO4, NaIO4, 10percent KHCO3 / acetonitrile / Ambient temperature
With
1H-imidazole; sodium periodate; copper(l) iodide; osmium(VIII) oxide; tetrabutylammomium bromide; sodium hydride; potassium hydrogencarbonate;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0040-4039(94)88291-6
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 86 percent / NaH, Bu4NBr / tetrahydrofuran / Ambient temperature
2: 100 percent / imidazole / dimethylformamide / Ambient temperature
3: 85 percent / OsO4, NaIO4, 10percent KHCO3 / acetonitrile / Ambient temperature
With
1H-imidazole; sodium periodate; osmium(VIII) oxide; tetrabutylammomium bromide; sodium hydride; potassium hydrogencarbonate;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0040-4039(94)88291-6
