(2S)-N-hydroxy-2-[(4-methoxybenzyl)oxy]-2-phenylethanimidoyl chloride

Base Information

• Chemical Name: (2S)-N-hydroxy-2-[(4-methoxybenzyl)oxy]-2-phenylethanimidoyl chloride
• CAS No.: 1134630-86-6
• Molecular Formula: C₁₆H₁₆ClNO₃
• Molecular Weight: 305.761

Synonyms:(2S)-N-hydroxy-2-[(4-methoxybenzyl)oxy]-2-phenylethanimidoyl chloride

Chemical Property of (2S)-N-hydroxy-2-[(4-methoxybenzyl)oxy]-2-phenylethanimidoyl chloride

Chemical Property:

Purity/Quality:

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Technology Process of (2S)-N-hydroxy-2-[(4-methoxybenzyl)oxy]-2-phenylethanimidoyl chloride

There total 1 articles about (2S)-N-hydroxy-2-[(4-methoxybenzyl)oxy]-2-phenylethanimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(2S)-[(4-methoxybenzyl)oxy](phenyl)acetaldehyde oxime (1134630-85-5) → (2S)-N-hydroxy-2-[(4-methoxybenzyl)oxy]-2-phenylethanimidoyl chloride (1134630-86-6)

Guidance literature:

With pyridine; N-chloro-succinimide; In chloroform; at 22 ℃; for 1.5h;

DOI:10.1039/b814054e

Reference yield: 33.0%

(2S)-N-hydroxy-2-[(4-methoxybenzyl)oxy]-2-phenylethanimidoyl chloride (1134630-86-6) + fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) → 3'-{(S)-[(4-methoxybenzyl)oxy](phenyl)methyl}isoxazolo[4'5':1,9](C60-Ih)[5,6]fullerene

Guidance literature:

With sodium hydrogencarbonate; In toluene; at 22 - 50 ℃;

DOI:10.1039/b814054e

Reference yield: 8.0%

(2S)-N-hydroxy-2-[(4-methoxybenzyl)oxy]-2-phenylethanimidoyl chloride (1134630-86-6) + [5,6]fullerene-C70 (741268-81-5,741268-84-8,133227-82-4,133320-10-2,133320-11-3,133869-47-3,134054-62-9,134932-61-9,149820-05-3,149820-06-4,157903-26-9,175779-21-2,115383-22-7,958017-68-0,958017-71-5,958017-74-8,958017-77-1,958017-80-6,140630-87-1,140694-21-9,151716-50-6,157008-89-4,220062-79-3,220062-83-9) → 3'-{(S)-[(4-methoxybenzyl)oxy](phenyl)methyl}isoxazolo[4'5':8,25](C70-D5h(6))[5,6]fullerene + (f,sA/C)-3'-{(S)-[(4-methoxybenzyl)oxy](phenyl)methyl}isoxazolo[4'5':7,22](C70-D5h(6))[5,6]fullerene + 3'-{(S)-[(4-methoxybenzyl)oxy](phenyl)methyl}isoxazolo[4'5':25,8](C70-D5h(6))[5,6]fullerene

Guidance literature:

With sodium hydrogencarbonate; In toluene; at 100 ℃; for 65h;

DOI:10.1039/b814054e

upstream raw materials:

(2S)-[(4-methoxybenzyl)oxy](phenyl)acetaldehyde oxime

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