Technology Process of Pt2I2(CH3C6H4N(H)C)((C6H5)2PCH2P(C6H5)2)2(1+)*ClO4(1-)=(Pt2I2(CN(H)C6H4CH3)((C6H5)2PCH2P(C6H5)2)2)ClO4
There total 1 articles about Pt2I2(CH3C6H4N(H)C)((C6H5)2PCH2P(C6H5)2)2(1+)*ClO4(1-)=(Pt2I2(CN(H)C6H4CH3)((C6H5)2PCH2P(C6H5)2)2)ClO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
HClO4;
In
ethanol; dichloromethane;
under N2, to a suspn. of Pt2I2(CNC6H4CH3)(dppm)2 in CH2Cl2 is added ethanol and 70% HClO4, stirred; evapd. under reduced pressure, filtered, washed with acidified (70% HClO4) EtOH and hexane, recrystd. from CH2Cl2-acidified EtOH, vac. dried at 100°C; elem. anal.;
DOI:10.1021/om50006a006