4-[(2-{1-acetoxy-3-[(2-azido-3-methyl-pentanoyl)-(3-methyl-butyryloxymethyl)-amino]-4-methyl-pentyl}-thiazole-4-carbonyl)-amino]-2-methyl-5-phenyl-pentanoic acid

Base Information

• Chemical Name: 4-[(2-{1-acetoxy-3-[(2-azido-3-methyl-pentanoyl)-(3-methyl-butyryloxymethyl)-amino]-4-methyl-pentyl}-thiazole-4-carbonyl)-amino]-2-methyl-5-phenyl-pentanoic acid
• CAS No.: 1005192-34-6
• Molecular Formula: C₃₆H₅₂N₆O₈S
• Molecular Weight: 728.91

Synonyms:4-[(2-{1-acetoxy-3-[(2-azido-3-methyl-pentanoyl)-(3-methyl-butyryloxymethyl)-amino]-4-methyl-pentyl}-thiazole-4-carbonyl)-amino]-2-methyl-5-phenyl-pentanoic acid

Chemical Property of 4-[(2-{1-acetoxy-3-[(2-azido-3-methyl-pentanoyl)-(3-methyl-butyryloxymethyl)-amino]-4-methyl-pentyl}-thiazole-4-carbonyl)-amino]-2-methyl-5-phenyl-pentanoic acid

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Technology Process of 4-[(2-{1-acetoxy-3-[(2-azido-3-methyl-pentanoyl)-(3-methyl-butyryloxymethyl)-amino]-4-methyl-pentyl}-thiazole-4-carbonyl)-amino]-2-methyl-5-phenyl-pentanoic acid

There total 1 articles about 4-[(2-{1-acetoxy-3-[(2-azido-3-methyl-pentanoyl)-(3-methyl-butyryloxymethyl)-amino]-4-methyl-pentyl}-thiazole-4-carbonyl)-amino]-2-methyl-5-phenyl-pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C34H50N6O7S + acetic anhydride (108-24-7) → 4-[(2-{1-acetoxy-3-[(2-azido-3-methyl-pentanoyl)-(3-methyl-butyryloxymethyl)-amino]-4-methyl-pentyl}-thiazole-4-carbonyl)-amino]-2-methyl-5-phenyl-pentanoic acid (1005192-34-6)

Guidance literature:

With pyridine; at 0 - 20 ℃; for 24h;

DOI:10.1002/chem.200701057

Reference yield: 77.0%

4-[(2-{1-acetoxy-3-[(2-azido-3-methyl-pentanoyl)-(3-methyl-butyryloxymethyl)-amino]-4-methyl-pentyl}-thiazole-4-carbonyl)-amino]-2-methyl-5-phenyl-pentanoic acid (1005192-34-6) + pentafluorophenyl acetate (19220-93-0) → 4-[(2-{1-acetoxy-3-[(2-acetylamino-3-methyl-pentanoyl)-(3-methyl-butyryloxymethyl)-amino]-4-methyl-pentyl}-thiazole-4-carbonyl)-amino]-2-methyl-5-phenyl-pentanoic acid (1005192-33-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 21h;

DOI:10.1002/chem.200701057

Reference yield: 48.0%

dimethylamino-acetic acid pentafluorophenyl ester (942919-64-4) + 4-[(2-{1-acetoxy-3-[(2-azido-3-methyl-pentanoyl)-(3-methyl-butyryloxymethyl)-amino]-4-methyl-pentyl}-thiazole-4-carbonyl)-amino]-2-methyl-5-phenyl-pentanoic acid (1005192-34-6) → 4-[(2-{1-acetoxy-3-[[2-(2-dimethylamino-acetylamino)-3-methyl-pentanoyl]-(3-methyl-butyryloxymethyl)-amino]-4-methyl-pentyl}-thiazole-4-carbonyl)-amino]-2-methyl-5-phenyl-pentanoic acid (1005192-32-4)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 26h;

DOI:10.1002/chem.200701057

upstream raw materials:

acetic anhydride

Downstream raw materials:

4-[(2-{1-acetoxy-3-[[2-(2-dimethylamino-acetylamino)-3-methyl-pentanoyl]-(3-methyl-butyryloxymethyl)-amino]-4-methyl-pentyl}-thiazole-4-carbonyl)-amino]-2-methyl-5-phenyl-pentanoic acid

4-[(2-{1-acetoxy-3-[(2-acetylamino-3-methyl-pentanoyl)-(3-methyl-butyryloxymethyl)-amino]-4-methyl-pentyl}-thiazole-4-carbonyl)-amino]-2-methyl-5-phenyl-pentanoic acid

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