methyl (6R,7E,10R,12Z)-6-acetoxy-10-(4-methoxybenzyloxy)-9-oxo-7,12-hexadecadienoate

Base Information

Chemical Name:methyl (6R,7E,10R,12Z)-6-acetoxy-10-(4-methoxybenzyloxy)-9-oxo-7,12-hexadecadienoate
CAS No.:1378240-27-7
Molecular Formula:C₂₇H₃₈O₇
Molecular Weight:474.595
Hs Code.:

Synonyms:methyl (6R,7E,10R,12Z)-6-acetoxy-10-(4-methoxybenzyloxy)-9-oxo-7,12-hexadecadienoate

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Chemical Property of methyl (6R,7E,10R,12Z)-6-acetoxy-10-(4-methoxybenzyloxy)-9-oxo-7,12-hexadecadienoate

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Technology Process of methyl (6R,7E,10R,12Z)-6-acetoxy-10-(4-methoxybenzyloxy)-9-oxo-7,12-hexadecadienoate

There total 8 articles about methyl (6R,7E,10R,12Z)-6-acetoxy-10-(4-methoxybenzyloxy)-9-oxo-7,12-hexadecadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1378240-26-6
methyl (R)-6-acetoxy-7-oxoheptanoate

: 1378240-24-4
dimethyl [(R)-3-(4-methoxybenzyloxy)-2-oxo-5-nonenyl]phosphonate

: 1378240-27-7
methyl (6R,7E,10R,12Z)-6-acetoxy-10-(4-methoxybenzyloxy)-9-oxo-7,12-hexadecadienoate

Guidance literature:: With triethylamine; lithium bromide; In tetrahydrofuran; at 20 ℃;
DOI:10.1271/bbb.110829

Reference yield:

: C₁₆H₂₂O₄

: 1378240-27-7
methyl (6R,7E,10R,12Z)-6-acetoxy-10-(4-methoxybenzyloxy)-9-oxo-7,12-hexadecadienoate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

2: n-butyllithium / tetrahydrofuran / -78 °C

3: triethylamine; lithium bromide / tetrahydrofuran / 20 °C

With dmap; n-butyllithium; triethylamine; dicyclohexyl-carbodiimide; lithium bromide; In tetrahydrofuran; dichloromethane;
DOI:10.1271/bbb.110829

Reference yield:

: 1378240-23-3
(2R,4Z)-N-methoxy-2-(4-methoxybenzyloxy)-N-methyl-4-octenamide

: 1378240-27-7
methyl (6R,7E,10R,12Z)-6-acetoxy-10-(4-methoxybenzyloxy)-9-oxo-7,12-hexadecadienoate

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran / -78 °C

2: triethylamine; lithium bromide / tetrahydrofuran / 20 °C

With n-butyllithium; triethylamine; lithium bromide; In tetrahydrofuran;
DOI:10.1271/bbb.110829