[Fe(FC₆H₄NNH)2(P(OC₂H₅)3)4]⁽²⁺⁾*2B(C₆H₅)4^(1-) = [Fe(FC₆H₄NNH)2(P(OC₂H₅)3)4](B(C₆H₅)4)2

Base Information

• Chemical Name: [Fe(FC₆H₄NNH)2(P(OC₂H₅)3)4]⁽²⁺⁾*2B(C₆H₅)4^(1-) = [Fe(FC₆H₄NNH)2(P(OC₂H₅)3)4](B(C₆H₅)4)2
• CAS No.: 103835-91-2
• Molecular Formula: 2C₂₄H₂₀B*C₃₆H₇₀F₂FeN₄O₁₂P₄
• Molecular Weight: 1607.18

Synonyms:[Fe(FC₆H₄NNH)2(P(OC₂H₅)3)4]⁽²⁺⁾*2B(C₆H₅)4^(1-) = [Fe(FC₆H₄NNH)2(P(OC₂H₅)3)4](B(C₆H₅)4)2

Chemical Property of [Fe(FC₆H₄NNH)2(P(OC₂H₅)3)4]⁽²⁺⁾*2B(C₆H₅)4^(1-) = [Fe(FC₆H₄NNH)2(P(OC₂H₅)3)4](B(C₆H₅)4)2

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Technology Process of [Fe(FC₆H₄NNH)2(P(OC₂H₅)3)4]⁽²⁺⁾*2B(C₆H₅)4^(1-) = [Fe(FC₆H₄NNH)2(P(OC₂H₅)3)4](B(C₆H₅)4)2

There total 2 articles about [Fe(FC₆H₄NNH)2(P(OC₂H₅)3)4]⁽²⁺⁾*2B(C₆H₅)4^(1-) = [Fe(FC₆H₄NNH)2(P(OC₂H₅)3)4](B(C₆H₅)4)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[FeH(FC6H4NNH)(P(OC2H5)3)4](1+)*B(C6H5)4(1-) = [FeH(FC6H4NNH)(P(OC2H5)3)4]B(C6H5)4 (103835-85-4) + sodium tetraphenyl borate (143-66-8) + 4-fluorobenzenediazonium tetrafluoroborate (459-45-0) → [Fe(FC6H4NNH)2(P(OC2H5)3)4](2+)*2B(C6H5)4(1-) = [Fe(FC6H4NNH)2(P(OC2H5)3)4](B(C6H5)4)2 (103835-91-2)

Guidance literature:

In dichloromethane; inert atmosphere; excess of diazonium salt; stirring for 1 h at 0°C; filtration; evapn. of solvent; addn. of ethanol containing NaBPh4; crystn. from CH2Cl2/ethanol; elem. anal.;

DOI:10.1021/ja00281a029

Reference yield:

FeH2(P(OC2H5)3)4 (34503-40-7) + sodium tetraphenyl borate (143-66-8) + 4-fluorobenzenediazonium tetrafluoroborate (459-45-0) → [FeH(FC6H4NNH)(P(OC2H5)3)4](1+)*B(C6H5)4(1-) = [FeH(FC6H4NNH)(P(OC2H5)3)4]B(C6H5)4 (103835-85-4) + [Fe(FC6H4NNH)2(P(OC2H5)3)4](2+)*2B(C6H5)4(1-) = [Fe(FC6H4NNH)2(P(OC2H5)3)4](B(C6H5)4)2 (103835-91-2)

Guidance literature:

In dichloromethane; inert atmosphere; excess of diazonium salt; -80°C; stirring for 10 min; warming to 0°C in 10-15 min; filtration; removal of solvent (reduced pressure); addn. of ethanol; addn. of NaBPh4; fractional crystn.; extn. of monodiazene complex by diethyl ether; removal of solvent (reduced pressure); crystn. with ethanol; sepn. of bis(diazene) complex by dissolving the residue in CH2Cl2; filtration; addn. ofethanol; total yield 80%; elem. anal.;

DOI:10.1021/ja00281a029

Reference yield:

[Fe(FC6H4NNH)2(P(OC2H5)3)4](2+)*2B(C6H5)4(1-) = [Fe(FC6H4NNH)2(P(OC2H5)3)4](B(C6H5)4)2 (103835-91-2) → [Fe(FC6H4NN)(P(OC2H5)3)4](1+)*B(C6H5)4(1-) = [Fe(FC6H4NN)(P(OC2H5)3)4]B(C6H5)4 (103835-99-0)

Guidance literature:

With triethyl amine; In dichloromethane; byproducts: ((C2H5)3NH)B(C6H5)4; inert atmosphere; 30 min; filtration; evapn.; addn. of ethanol; removal of solid by filtration; slow cooling to -30°C; elem. anal.;

DOI:10.1021/ja00281a029

upstream raw materials:

[FeH(FC₆H₄NNH)(P(OC₂H₅)3)4]⁽¹⁺⁾*B(C₆H₅)4^(1-) = [FeH(FC₆H₄NNH)(P(OC₂H₅)3)4]B(C₆H₅)4

sodium tetraphenyl borate

4-fluorobenzenediazonium tetrafluoroborate

FeH₂(P(OC₂H₅)3)4

Downstream raw materials:

[Fe(FC₆H₄NN)(P(OC₂H₅)3)4]⁽¹⁺⁾*B(C₆H₅)4^(1-) = [Fe(FC₆H₄NN)(P(OC₂H₅)3)4]B(C₆H₅)4

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