C₂₄H₃₈O₆Si

Base Information

Chemical Name:C₂₄H₃₈O₆Si
CAS No.:1313484-60-4
Molecular Formula:C₂₄H₃₈O₆Si
Molecular Weight:450.648
Hs Code.:

C<sub>24</sub>H<sub>38</sub>O<sub>6</sub>Si

Synonyms:C₂₄H₃₈O₆Si

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Chemical Property of C₂₄H₃₈O₆Si

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Technology Process of C₂₄H₃₈O₆Si

There total 9 articles about C₂₄H₃₈O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 874-61-3
4-oxocyclohexanecarboxylic acid

: 1313484-40-0
C₁₇H₃₀O₄Si

: 1313484-60-4
C₂₄H₃₈O₆Si

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1039/c1cc11388g

Reference yield:

: C₁₆H₂₄O₅

: 1313484-60-4
C₂₄H₃₈O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1: 1H-imidazole; sodium hydrogencarbonate / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere

2: trifluoroacetic acid / water / 0.5 h / 20 °C / Inert atmosphere

3: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

4: Grubbs catalyst first generation / dichloromethane / 18 h / 20 °C / Inert atmosphere

5: pyridine hydrogenfluoride / tetrahydrofuran / 20 h / 0 - 20 °C / Inert atmosphere

6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C

With 1H-imidazole; Grubbs catalyst first generation; dmap; sodium hydrogencarbonate; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 1: Baylis-Hillman reaction;
DOI:10.1039/c1cc11388g

Reference yield:

: 1313484-52-4
C₁₆H₂₄O₅

: 1313484-60-4
C₂₄H₃₈O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1: dichloro bis(acetonitrile) palladium(II) / toluene / 47 h / 65 °C / Inert atmosphere

2: 1H-imidazole; sodium hydrogencarbonate / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere

3: trifluoroacetic acid / water / 0.5 h / 20 °C / Inert atmosphere

4: 1H-imidazole / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

5: Grubbs catalyst first generation / dichloromethane / 18 h / 20 °C / Inert atmosphere

6: pyridine hydrogenfluoride / tetrahydrofuran / 20 h / 0 - 20 °C / Inert atmosphere

7: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C

With 1H-imidazole; Grubbs catalyst first generation; dmap; dichloro bis(acetonitrile) palladium(II); sodium hydrogencarbonate; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene; 2: Baylis-Hillman reaction;
DOI:10.1039/c1cc11388g