Benzoic acid (1S,2S,4R)-2-azido-4-hydroxymethyl-cyclopentylmethyl ester

Base Information

Chemical Name:Benzoic acid (1S,2S,4R)-2-azido-4-hydroxymethyl-cyclopentylmethyl ester
CAS No.:116142-72-4
Molecular Formula:C₁₄H₁₇N₃O₃
Molecular Weight:275.307
Hs Code.:

Synonyms:Benzoic acid (1S,2S,4R)-2-azido-4-hydroxymethyl-cyclopentylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid (1S,2S,4R)-2-azido-4-hydroxymethyl-cyclopentylmethyl ester

Chemical Property:

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Technology Process of Benzoic acid (1S,2S,4R)-2-azido-4-hydroxymethyl-cyclopentylmethyl ester

There total 2 articles about Benzoic acid (1S,2S,4R)-2-azido-4-hydroxymethyl-cyclopentylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116142-71-3
Benzoic acid (1R,2R,4R)-4-hydroxymethyl-2-methanesulfonyloxy-cyclopentylmethyl ester

: 116142-72-4
Benzoic acid (1S,2S,4R)-2-azido-4-hydroxymethyl-cyclopentylmethyl ester

Guidance literature:: With sodium azide; In dimethyl sulfoxide; at 40 ℃; Yield given;
DOI:10.1016/S0040-4039(00)96716-9

Reference yield:

: 116142-70-2
(-)-(1R,2R,4R)-2-<(benzoyloxy)methyl>-4-<(benzyloxy)methyl>cyclopentyl methanesulfonate

: 116142-72-4
Benzoic acid (1S,2S,4R)-2-azido-4-hydroxymethyl-cyclopentylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 5percent Pd/C / ethanol / 5 h

2: NaN₃ / dimethylsulfoxide / 40 °C

With sodium azide; hydrogen; palladium on activated charcoal; In ethanol; dimethyl sulfoxide;
DOI:10.1016/S0040-4039(00)96716-9