2-Phenylethylamine Hydroiodide

Base Information

• Chemical Name: 2-Phenylethylamine Hydroiodide
• CAS No.: 151059-43-7
• Molecular Formula: C₈H₁₂N*I
• Molecular Weight: 249.094
• Mol file: 151059-43-7.mol

Synonyms:2-phenylethan-1-ammonium Iodide

Chemical Property of 2-Phenylethylamine Hydroiodide

Chemical Property:

• Melting Point: 267 °C
• Storage Temp.: Hygroscopic, Refrigerator, under inert atmosphere
• Solubility.: DMSO (Slightly), Methanol (Slightly)

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-Phenylethylamine Hydroiodide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 2-Phenylethylamine Hydroiodide can be used in the post-treatment of perovskite films for hysteresis-less perovskite solar cells.

Technology Process of 2-Phenylethylamine Hydroiodide

There total 3 articles about 2-Phenylethylamine Hydroiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-phenethyl iodide (17376-04-4) → 2-phenylethan-1-ammonium Iodide (151059-43-7)

Guidance literature:

With ammonium hydroxide; In methanol; at 160 ℃; for 0.166667h; under 18100.7 Torr; chemoselective reaction; Flow reactor;

DOI:10.1021/acs.joc.8b02387

Reference yield: 83.0%

phenethylamine (64-04-0) → 2-phenylethan-1-ammonium Iodide (151059-43-7)

Guidance literature:

With hydrogen iodide; In ethanol; water;

DOI:10.1021/jacs.5b11740

Reference yield:

2-phenethyl iodide (17376-04-4) → 2-phenylethan-1-ammonium Iodide (151059-43-7) + diphenethylamine (6308-98-1)

Guidance literature:

With ammonia; In methanol; at 130 ℃; for 0.5h; microwave irradiation;

DOI:10.1016/j.tetlet.2003.10.146

upstream raw materials:

2-phenethyl iodide

phenethylamine

Refernces

• 1、 Liao, Yuqin,Liu, Hefei,Zhou, Wenjia,Yang, Dongwen,Shang, Yuequn,Shi, Zhifang,Li, Binghan,Jiang, Xianyuan,Zhang, Lijun,Quan, Li Na,Quintero-Bermudez, Rafael,Sutherland, Brandon R.,Mi, Qixi,Sargent, Edward H.,Ning, Zhijun. "Highly Oriented Low-Dimensional Tin Halide Perovskites with Enhanced Stability and Photovoltaic Performance". . p. 6693 - 6699. Retrieved 2017.
• 2、 Quan, Li Na,Yuan, Mingjian,Comin, Riccardo,Voznyy, Oleksandr,Beauregard, Eric M.,Hoogland, Sjoerd,Buin, Andrei,Kirmani, Ahmad R.,Zhao, Kui,Amassian, Aram,Kim, Dong Ha,Sargent, Edward H.. "Ligand-Stabilized Reduced-Dimensionality Perovskites". . p. 2649 - 2655. Retrieved 2016.
• 3、 Herckens, Roald,Van Gompel, Wouter T. M.,Song, Wenya,Gélvez-Rueda, María C.,Maufort, Arthur,Ruttens, Bart,D'Haen, Jan,Grozema, Ferdinand C.,Aernouts, Tom,Lutsen, Laurence,Vanderzande, Dirk. "Multi-layered hybrid perovskites templated with carbazole derivatives: Optical properties, enhanced moisture stability and solar cell characteristics". . p. 22899 - 22908. Retrieved 2018/11/27.