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Technology Process of bis[(3R)-1-phenyl-4,4-dimethyl-2-oxopyrrolidin-3-yl] (1S,3S,5S,7S)-5,7-diiodotricyclo[3.3.0.03,7]octane-1,3-dicarboxylate

bis[(3R)-1-phenyl-4,4-dimethyl-2-oxopyrrolidin-3-yl] (1S,3S,5S,7S)-5,7-diiodotricyclo[3.3.0.03,7]octane-1,3-dicarboxylate

Base Information
  • Chemical Name:bis[(3R)-1-phenyl-4,4-dimethyl-2-oxopyrrolidin-3-yl] (1S,3S,5S,7S)-5,7-diiodotricyclo[3.3.0.03,7]octane-1,3-dicarboxylate
  • CAS No.:949091-74-1
  • Molecular Formula:C34H36I2N2O6
  • Molecular Weight:822.479
  • Hs Code.:
bis[(3R)-1-phenyl-4,4-dimethyl-2-oxopyrrolidin-3-yl] (1S,3S,5S,7S)-5,7-diiodotricyclo[3.3.0.0<sup>3,7</sup>]octane-1,3-dicarboxylate

Synonyms:bis[(3R)-1-phenyl-4,4-dimethyl-2-oxopyrrolidin-3-yl] (1S,3S,5S,7S)-5,7-diiodotricyclo[3.3.0.03,7]octane-1,3-dicarboxylate

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Chemical Property of bis[(3R)-1-phenyl-4,4-dimethyl-2-oxopyrrolidin-3-yl] (1S,3S,5S,7S)-5,7-diiodotricyclo[3.3.0.03,7]octane-1,3-dicarboxylate
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Technology Process of bis[(3R)-1-phenyl-4,4-dimethyl-2-oxopyrrolidin-3-yl] (1S,3S,5S,7S)-5,7-diiodotricyclo[3.3.0.03,7]octane-1,3-dicarboxylate

There total 1 articles about bis[(3R)-1-phenyl-4,4-dimethyl-2-oxopyrrolidin-3-yl] (1S,3S,5S,7S)-5,7-diiodotricyclo[3.3.0.03,7]octane-1,3-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

(+/-)-(1S,3S,5S,7S)-5,7-diiodotricyclo[3.3.0.0<sup>3,7</sup>]octane-1,3-dicarboxylic acid

(+/-)-(1S,3S,5S,7S)-5,7-diiodotricyclo[3.3.0.03,7]octane-1,3-dicarboxylic acid

(R)-3-hydroxy-4,4-dimethyl-1-phenylpyrrolidin-2-one
169221-13-0

(R)-3-hydroxy-4,4-dimethyl-1-phenylpyrrolidin-2-one

bis[(3R)-1-phenyl-4,4-dimethyl-2-oxopyrrolidin-3-yl] (1R,3R,5R,7R)-5,7-diiodotricyclo[3.3.0.0<sup>3,7</sup>]octane-1,3-dicarboxylate
949091-73-0

bis[(3R)-1-phenyl-4,4-dimethyl-2-oxopyrrolidin-3-yl] (1R,3R,5R,7R)-5,7-diiodotricyclo[3.3.0.03,7]octane-1,3-dicarboxylate

bis[(3R)-1-phenyl-4,4-dimethyl-2-oxopyrrolidin-3-yl] (1S,3S,5S,7S)-5,7-diiodotricyclo[3.3.0.0<sup>3,7</sup>]octane-1,3-dicarboxylate
949091-74-1

bis[(3R)-1-phenyl-4,4-dimethyl-2-oxopyrrolidin-3-yl] (1S,3S,5S,7S)-5,7-diiodotricyclo[3.3.0.03,7]octane-1,3-dicarboxylate

Guidance literature:
With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 21h;
DOI:10.1016/j.tet.2007.05.061
upstream raw materials:

(R)-3-hydroxy-4,4-dimethyl-1-phenylpyrrolidin-2-one

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