1-acetyl-α-<methyl>-2,3-dihydro-1H-indole-5-methanol acetate ester

Base Information

Chemical Name:1-acetyl-α-<methyl>-2,3-dihydro-1H-indole-5-methanol acetate ester
CAS No.:101544-40-5
Molecular Formula:C₂₈H₃₀N₂O₃
Molecular Weight:442.558
Hs Code.:

1-acetyl-α-<<bis(phenylmethyl)amino>methyl>-2,3-dihydro-1H-indole-5-methanol acetate ester

Synonyms:1-acetyl-α-<methyl>-2,3-dihydro-1H-indole-5-methanol acetate ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-acetyl-α-<methyl>-2,3-dihydro-1H-indole-5-methanol acetate ester

Chemical Property:

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Technology Process of 1-acetyl-α-<methyl>-2,3-dihydro-1H-indole-5-methanol acetate ester

There total 5 articles about 1-acetyl-α-<methyl>-2,3-dihydro-1H-indole-5-methanol acetate ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.5%

: 108-24-7
acetic anhydride

: 101544-39-2
1-acetyl-2,3-dihydro-α-<methyl>-1H-indole-5-methanol

: 101544-40-5
1-acetyl-α-<methyl>-2,3-dihydro-1H-indole-5-methanol acetate ester

Guidance literature:: With pyridine; Ambient temperature;
DOI:10.1021/jm00156a019

Reference yield:

: 101544-39-2
1-acetyl-2,3-dihydro-α-<methyl>-1H-indole-5-methanol

: 101544-40-5
1-acetyl-α-<methyl>-2,3-dihydro-1H-indole-5-methanol acetate ester

Guidance literature:: With pyridine; In dichloromethane; acetic anhydride;

Reference yield:

: 16078-30-1
1-Acetyl-2,3-dihydro-1H-indole

: 101544-40-5
1-acetyl-α-<methyl>-2,3-dihydro-1H-indole-5-methanol acetate ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) aluminum chloride / 1.) 1,2-dichloroethane, 20 min, 2.) 1,2-dichloroethane, 50 deg C, 1 h

2: dimethylformamide / 2 h / 60 °C

3: NaBH₄ / ethanol / 1.) RT, 4.5 h, 2.) 50 deg C, 1 h

4: 94.5 percent / pyridine / Ambient temperature

With pyridine; sodium tetrahydroborate; aluminium trichloride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00156a019