1-benzyl-4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

Base Information

Chemical Name:1-benzyl-4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide
CAS No.:1312698-79-5
Molecular Formula:C₁₆H₁₅N₅OS₂
Molecular Weight:357.46
Hs Code.:

Synonyms:1-benzyl-4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

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Chemical Property of 1-benzyl-4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

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Technology Process of 1-benzyl-4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

There total 4 articles about 1-benzyl-4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1073-62-7,20570-96-1
N-benzylhydrazine hydrochloride

: 5-(4-isothiocyanatophenyl)-1,3,4-oxadiazole-2-thiol

: 1312698-79-5
1-benzyl-4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

Guidance literature:: In toluene; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.04.017

Reference yield:

: 619-45-4
4-methoxycarbonyl aniline

: 1312698-79-5
1-benzyl-4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrazine hydrate / 1 h / Reflux

2.1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 0 °C / Inert atmosphere; Reflux

2.2: pH 4

3.1: sodium hydrogencarbonate / acetone / 0.5 h / 0 - 20 °C

4.1: toluene / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; hydrazine hydrate; potassium hydroxide; In ethanol; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.ejmech.2011.04.017

Reference yield:

: 5351-17-7
4-aminobenzohydrazide

: 1312698-79-5
1-benzyl-4-(4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 0 °C / Inert atmosphere; Reflux

1.2: pH 4

2.1: sodium hydrogencarbonate / acetone / 0.5 h / 0 - 20 °C

3.1: toluene / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; potassium hydroxide; In ethanol; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.ejmech.2011.04.017