4-[4-(N,N-dimethylamino)styryl]-2,5-diphenylbenzaldehyde

Base Information

Chemical Name:4-[4-(N,N-dimethylamino)styryl]-2,5-diphenylbenzaldehyde
CAS No.:1300701-04-5
Molecular Formula:C₂₉H₂₅NO
Molecular Weight:403.524
Hs Code.:

Synonyms:4-[4-(N,N-dimethylamino)styryl]-2,5-diphenylbenzaldehyde

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Chemical Property of 4-[4-(N,N-dimethylamino)styryl]-2,5-diphenylbenzaldehyde

Chemical Property:

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Technology Process of 4-[4-(N,N-dimethylamino)styryl]-2,5-diphenylbenzaldehyde

There total 3 articles about 4-[4-(N,N-dimethylamino)styryl]-2,5-diphenylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 144836-60-2
[1,1':4',1]-terphenyl-2',5'-dicarbaldehyde

: 34904-03-5
4-(N,N-dimethylamino)benzyltriphenylphosphonium iodide

: 1300701-04-5
4-[4-(N,N-dimethylamino)styryl]-2,5-diphenylbenzaldehyde

Guidance literature:: With potassium tert-butylate; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2011.03.108

Reference yield:

: 106-42-3
para-xylene

: 1300701-04-5
4-[4-(N,N-dimethylamino)styryl]-2,5-diphenylbenzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: bromine / tetrachloromethane

1.2: Irradiation

2.1: water; silver nitrate / ethanol

3.1: palladium diacetate; sodium carbonate; triphenylphosphine / water; isopropyl alcohol / 4 h / 70 °C

4.1: potassium tert-butylate / dichloromethane / 2 h / 20 °C

With potassium tert-butylate; water; bromine; palladium diacetate; sodium carbonate; silver nitrate; triphenylphosphine; In tetrachloromethane; ethanol; dichloromethane; water; isopropyl alcohol; 3.1: Suzuki coupling / 4.1: Wittig reaction;
DOI:10.1016/j.tet.2011.03.108

Reference yield:

: 36711-69-0
1,4-dibromo-2,5-bis(dibromomethyl)benzene

: 1300701-04-5
4-[4-(N,N-dimethylamino)styryl]-2,5-diphenylbenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: water; silver nitrate / ethanol

2: palladium diacetate; sodium carbonate; triphenylphosphine / water; isopropyl alcohol / 4 h / 70 °C

3: potassium tert-butylate / dichloromethane / 2 h / 20 °C

With potassium tert-butylate; water; palladium diacetate; sodium carbonate; silver nitrate; triphenylphosphine; In ethanol; dichloromethane; water; isopropyl alcohol; 2: Suzuki coupling / 3: Wittig reaction;
DOI:10.1016/j.tet.2011.03.108