C₈H₁₃N₃O

Base Information

• Chemical Name: C₈H₁₃N₃O
• CAS No.: 1624363-26-3
• Molecular Formula: C₈H₁₃N₃O
• Molecular Weight: 167.211
• Mol file: 1624363-26-3.mol

Synonyms:C₈H₁₃N₃O

Chemical Property of C₈H₁₃N₃O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₈H₁₃N₃O

There total 2 articles about C₈H₁₃N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

1-Ethynylcyclohexan-1-ol (78-27-3) → C8H13N3O (1624363-26-3)

Guidance literature:

With trimethylsilylazide; silver carbonate; In dimethyl sulfoxide; at 80 ℃; chemoselective reaction;

DOI:10.1002/anie.201310264

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → C8H13N3O (1624363-26-3)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 3 h / 0 - 60 °C / Inert atmosphere

2: trimethylsilylazide; water; silver carbonate / dimethyl sulfoxide / 2 h / 80 °C

With trimethylsilylazide; water; silver carbonate; In tetrahydrofuran; dimethyl sulfoxide;

DOI:10.1021/acs.orglett.1c01062

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + C8H13N3O (1624363-26-3) → C13H21N3O3

Guidance literature:

With dmap; triethylamine; In 1,2-dichloro-ethane; at 20 ℃; for 12h;

DOI:10.1002/ejoc.201901699

upstream raw materials:

1-Ethynylcyclohexan-1-ol

cyclohexanone