5,6-dideoxy-1,2-O-isopropylidene-3-O-p-tolylsulfonyl-α-D-ribo-hex-5-enofuranose

Base Information

Chemical Name:5,6-dideoxy-1,2-O-isopropylidene-3-O-p-tolylsulfonyl-α-D-ribo-hex-5-enofuranose
CAS No.:88238-34-0
Molecular Formula:C₁₆H₂₀O₆S
Molecular Weight:340.397
Hs Code.:

Synonyms:5,6-dideoxy-1,2-O-isopropylidene-3-O-p-tolylsulfonyl-α-D-ribo-hex-5-enofuranose

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Chemical Property of 5,6-dideoxy-1,2-O-isopropylidene-3-O-p-tolylsulfonyl-α-D-ribo-hex-5-enofuranose

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 5,6-dideoxy-1,2-O-isopropylidene-3-O-p-tolylsulfonyl-α-D-ribo-hex-5-enofuranose

There total 3 articles about 5,6-dideoxy-1,2-O-isopropylidene-3-O-p-tolylsulfonyl-α-D-ribo-hex-5-enofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 7022-86-8,52625-60-2,88238-33-9
1,2-O-isopropylidene-3,5,6-tri-O-p-tolylsulfonyl-α-D-allofuranose

: 88238-34-0
5,6-dideoxy-1,2-O-isopropylidene-3-O-p-tolylsulfonyl-α-D-ribo-hex-5-enofuranose

Guidance literature:: With sodium iodide; In butanone; for 18h; Heating;
DOI:10.1016/0008-6215(83)84009-9

Reference yield:

: 620630-82-2
1,2 5,6-O-di(isopropylidene)-α-D-allofuranose

: 88238-34-0
5,6-dideoxy-1,2-O-isopropylidene-3-O-p-tolylsulfonyl-α-D-ribo-hex-5-enofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 70percent aq. acetic acid / 16 h / Ambient temperature

2: 85.8 percent / pyridine / 96 h / Ambient temperature

3: 83 percent / NaI / butan-2-one / 18 h / Heating

With acetic acid; sodium iodide; In pyridine; butanone;
DOI:10.1016/0008-6215(83)84009-9

Reference yield:

: 582-51-4,4495-04-9,18549-40-1,27108-10-7,29747-91-9,31718-77-1,51921-42-7,121701-18-6
1,2-O-isopropylidene-α-D-allofuranose

: 88238-34-0
5,6-dideoxy-1,2-O-isopropylidene-3-O-p-tolylsulfonyl-α-D-ribo-hex-5-enofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 85.8 percent / pyridine / 96 h / Ambient temperature

2: 83 percent / NaI / butan-2-one / 18 h / Heating

With sodium iodide; In pyridine; butanone;
DOI:10.1016/0008-6215(83)84009-9