Technology Process of C44H61BrN2O5
There total 8 articles about C44H61BrN2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
carbon tetrabromide; triphenylphosphine;
In
tetrahydrofuran;
Inert atmosphere;
DOI:10.1039/c0ob01034k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
2: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / Inert atmosphere
With
lithium aluminium tetrahydride; carbon tetrabromide; triphenylphosphine;
In
tetrahydrofuran;
DOI:10.1039/c0ob01034k
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium tetrahydroborate / tetrahydrofuran; methanol
2.1: triethylamine / chloroform / 0.08 h / Inert atmosphere
2.2: 24 h / Inert atmosphere
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
5.1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / Inert atmosphere
With
sodium tetrahydroborate; lithium aluminium tetrahydride; carbon tetrabromide; triethylamine; triphenylphosphine;
In
tetrahydrofuran; methanol; chloroform;
DOI:10.1039/c0ob01034k