toluene-4-sulfonic acid 2-(2-{5-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethyl ester

Base Information

• Chemical Name: toluene-4-sulfonic acid 2-(2-{5-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethyl ester
• CAS No.: 603131-41-5
• Molecular Formula: C₆₀H₆₈O₈S
• Molecular Weight: 949.261
• Mol file: 603131-41-5.mol

Synonyms:toluene-4-sulfonic acid 2-(2-{5-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethyl ester

Chemical Property of toluene-4-sulfonic acid 2-(2-{5-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of toluene-4-sulfonic acid 2-(2-{5-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethyl ester

There total 1 articles about toluene-4-sulfonic acid 2-(2-{5-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2-(2-{5-[2-(2-toluene-4-sulfonyloxy-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethoxysulfonyl-4-toluene (153530-55-3) + bis(4-tert-butylphenyl)(4-ethylphenyl)(4-hydroxyphenyl)methane (177609-49-3) → toluene-4-sulfonic acid 2-(2-{5-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethyl ester (603131-41-5)

Guidance literature:

With potassium carbonate; In acetonitrile; for 84h; Heating;

DOI:10.1002/chem.200204589

Reference yield: 90.0%

1,4-bis[2-(4-hydroxyphenyl)-2-propylene]benzene (4084-45-1) + toluene-4-sulfonic acid 2-(2-{5-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethyl ester (603131-41-5) → C124H134O12

Guidance literature:

With 18-crown-6 ether; potassium carbonate; lithium bromide; In N,N-dimethyl-formamide; at 100 ℃; for 10h;

DOI:10.1002/chem.200305725

Reference yield: 87.0%

2-(2-{5-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethanol (346701-88-0) + toluene-4-sulfonic acid 2-(2-{5-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethyl ester (603131-41-5) → TIMEOUT: 5s

Guidance literature:

2-(2-{5-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethanol; With sodium hydride; In tetrahydrofuran; for 30h; Heating;

toluene-4-sulfonic acid 2-(2-{5-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethyl ester; In tetrahydrofuran; for 16h; Heating;

DOI:10.1002/chem.200305725

upstream raw materials:

2-(2-{5-[2-(2-toluene-4-sulfonyloxy-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethoxysulfonyl-4-toluene

bis(4-tert-butylphenyl)(4-ethylphenyl)(4-hydroxyphenyl)methane

Downstream raw materials:

2-{4-[2-(2-{5-[2-(2-{4-[bis-(4-tert-butyl-phenyl)-(4-ethyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-naphthalen-1-yloxy}-ethoxy)-ethylsulfanyl]-5-ethylsulfanyl-[1,3]dithiol-2-ylidene}-5H-[1,3]dithiolo[4,5-c]pyrrole