2β-[3-benzoyloxy-1α-(4-methoxy-benzyloxy)-propyl]-5β-isopropyl-2α-methyl-cyclohexanone

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Chemical Name:2β-[3-benzoyloxy-1α-(4-methoxy-benzyloxy)-propyl]-5β-isopropyl-2α-methyl-cyclohexanone
CAS No.:741259-09-6
Molecular Formula:C₂₈H₃₆O₅
Molecular Weight:452.591
Hs Code.:

Synonyms:2β-[3-benzoyloxy-1α-(4-methoxy-benzyloxy)-propyl]-5β-isopropyl-2α-methyl-cyclohexanone

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Chemical Property of 2β-[3-benzoyloxy-1α-(4-methoxy-benzyloxy)-propyl]-5β-isopropyl-2α-methyl-cyclohexanone

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Technology Process of 2β-[3-benzoyloxy-1α-(4-methoxy-benzyloxy)-propyl]-5β-isopropyl-2α-methyl-cyclohexanone

There total 3 articles about 2β-[3-benzoyloxy-1α-(4-methoxy-benzyloxy)-propyl]-5β-isopropyl-2α-methyl-cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 89238-99-3
O-(4-methoxybenzyl)-trichloroacetimidate

: 741259-07-4
2β-(3-benzoyloxy-1α-hydroxy-propyl)-5β-isopropyl-2α-methyl-cyclohexanone

: 741259-09-6
2β-[3-benzoyloxy-1α-(4-methoxy-benzyloxy)-propyl]-5β-isopropyl-2α-methyl-cyclohexanone

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2004.05.056

Reference yield:

: 6485-40-1,2244-16-8
(R)-Carvone

: 741259-09-6
2β-[3-benzoyloxy-1α-(4-methoxy-benzyloxy)-propyl]-5β-isopropyl-2α-methyl-cyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: H₂ / Pd/C / ethanol / 30 h

1.2: 90 percent / NEt₃ / dimethylformamide / 48 h / Heating

2.1: 670 mg / TiCl₄ / CH₂Cl₂ / -78 - -40 °C

3.1: 85 percent / p-TsOH / CH₂Cl₂ / 24 h / 20 °C

With hydrogen; titanium tetrachloride; toluene-4-sulfonic acid; palladium on activated charcoal; In ethanol; dichloromethane; 2.1: Mukaiyama aldol reaction;
DOI:10.1016/j.tet.2004.05.056

Reference yield:

: 99058-97-6
3-oxopropyl benzoate

: 741259-09-6
2β-[3-benzoyloxy-1α-(4-methoxy-benzyloxy)-propyl]-5β-isopropyl-2α-methyl-cyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: 670 mg / TiCl₄ / CH₂Cl₂ / -78 - -40 °C

2: 85 percent / p-TsOH / CH₂Cl₂ / 24 h / 20 °C

With titanium tetrachloride; toluene-4-sulfonic acid; In dichloromethane; 1: Mukaiyama aldol reaction;
DOI:10.1016/j.tet.2004.05.056