[(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetrphenylporphyrinato)bis(tetrahydrofurane)iron(III)] perchlorate complex

Base Information

Chemical Name:[(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetrphenylporphyrinato)bis(tetrahydrofurane)iron(III)] perchlorate complex
CAS No.:313391-45-6
Molecular Formula:C₆₈H₇₆FeN₄O₂*ClO₄
Molecular Weight:1136.67
Hs Code.:

Synonyms:[(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetrphenylporphyrinato)bis(tetrahydrofurane)iron(III)] perchlorate complex

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Chemical Property of [(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetrphenylporphyrinato)bis(tetrahydrofurane)iron(III)] perchlorate complex

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Technology Process of [(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetrphenylporphyrinato)bis(tetrahydrofurane)iron(III)] perchlorate complex

There total 2 articles about [(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetrphenylporphyrinato)bis(tetrahydrofurane)iron(III)] perchlorate complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 953387-00-3,146343-96-6
(chloro)(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetrphenylporphyrinato)iron(III) complex

: silver perchlorate

: 313391-45-6
[(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetrphenylporphyrinato)bis(tetrahydrofurane)iron(III)] perchlorate complex

Guidance literature:: In tetrahydrofuran; byproducts: AgCl; THF soln. of AgClO4 was added to THF soln. of Fe-complex, stirred for 1 min at room temp.; evapd., CH2Cl2 was added, filtered, evapd., THF was added, heptane was added, allowed to stand overnight, filtered, washed with hexane, dried invacuo for 10 min at 25°C;
DOI:10.1021/ic001412b

Reference yield:

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: Fe(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetraphenylporphyrinato)ClO₄

: 313391-45-6
[(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetrphenylporphyrinato)bis(tetrahydrofurane)iron(III)] perchlorate complex

Guidance literature:: In dichloromethane-d2; a soln. of ligand added at ambient temp. to a soln. of Fe complex; not isolated, detected by NMR, ESR;
DOI:10.1021/ic0488942

Reference yield:

: 313391-45-6
[(2,3,7,8,12,13,17,18-octaethyl-5,10,15,20-tetrphenylporphyrinato)bis(tetrahydrofurane)iron(III)] perchlorate complex

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 953386-86-2
[(octaethyltetraphenylporphyrinato)Fe(tert-butylisocyanide)2]Cl

Guidance literature:: In dichloromethane; addn. of 6-10 equiv. of tert-butylisocyanide to CH2Cl2 soln. of iron compd. in NMR tube; not isolated, ESR;
DOI:10.1021/ic700827w