(E)-3-phenylacrylic acid 4'-[(E)-(3-phenylacryloyl)oxymethyl]-[2,2']bipyridinyl-4-ylmethyl ester

Base Information

Chemical Name:(E)-3-phenylacrylic acid 4'-[(E)-(3-phenylacryloyl)oxymethyl]-[2,2']bipyridinyl-4-ylmethyl ester
CAS No.:866789-01-7
Molecular Formula:C₃₀H₂₄N₂O₄
Molecular Weight:476.532
Hs Code.:

Synonyms:(E)-3-phenylacrylic acid 4'-[(E)-(3-phenylacryloyl)oxymethyl]-[2,2']bipyridinyl-4-ylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-phenylacrylic acid 4'-[(E)-(3-phenylacryloyl)oxymethyl]-[2,2']bipyridinyl-4-ylmethyl ester

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Technology Process of (E)-3-phenylacrylic acid 4'-[(E)-(3-phenylacryloyl)oxymethyl]-[2,2']bipyridinyl-4-ylmethyl ester

There total 1 articles about (E)-3-phenylacrylic acid 4'-[(E)-(3-phenylacryloyl)oxymethyl]-[2,2']bipyridinyl-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109073-77-0
4,4'-bis(hydroxymethyl)-2,2'-bipyridine

: 866789-01-7
(E)-3-phenylacrylic acid 4'-[(E)-(3-phenylacryloyl)oxymethyl]-[2,2']bipyridinyl-4-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 85 percent / diisopropylcarbodiimide / CH₂Cl₂; tetrahydrofuran / 0.33 h / 100 °C / microwave irradiation

2.1: t-BuOK / tetrahydrofuran / 0.25 h / 0 °C

2.2: 98 percent / tetrahydrofuran / 0 - 25 °C

With potassium tert-butylate; diisopropyl-carbodiimide; In tetrahydrofuran; dichloromethane; 2.2: Horner-Emmons reaction;
DOI:10.1039/b503778f

Reference yield: 95.0%

: 866789-01-7
(E)-3-phenylacrylic acid 4'-[(E)-(3-phenylacryloyl)oxymethyl]-[2,2']bipyridinyl-4-ylmethyl ester

: 103-26-4,1754-62-7
Methyl cinnamate

Guidance literature:: With triethylamine; In tetrahydrofuran; methanol; at 120 ℃; for 2h; microwave irradiation;
DOI:10.1039/b503778f

Reference yield: 92.0%

: 866789-01-7
(E)-3-phenylacrylic acid 4'-[(E)-(3-phenylacryloyl)oxymethyl]-[2,2']bipyridinyl-4-ylmethyl ester

: 78-93-3
butanone

: 384332-81-4
4-methyl-5-phenylcyclohexane-1,3-dione

Guidance literature:: butanone; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.333333h;

(E)-3-phenylacrylic acid 4'-[(E)-(3-phenylacryloyl)oxymethyl]-[2,2']bipyridinyl-4-ylmethyl ester; In tetrahydrofuran; at 70 ℃; for 0.75h; microwave irradiation;
DOI:10.1039/b503778f