4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one

Base Information

• Chemical Name: 4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one
• CAS No.: 97507-59-0
• Molecular Formula: C₁₄H₁₅N₃O
• Molecular Weight: 241.293

Synonyms:4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one

Chemical Property of 4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one

Chemical Property:

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Technology Process of 4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one

There total 24 articles about 4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

4,4-dimethyl-6-phenylazo-7-phthalimido-7-azabicyclo[4.1.0]heptan-2-one → 4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one (97507-59-0)

Guidance literature:

With trifluoroacetic acid; In chloroform; at 18 - 23 ℃;

DOI:10.1007/s10593-005-0319-9

Reference yield: 57.0%

C16H19N3O3 (103869-95-0) → 4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one (97507-59-0)

Guidance literature:

With sodium hydroxide; 5 min heating then EtOH, 5 min;

DOI:10.1002/hlca.19850680630

Reference yield: 52.0%

5,5-dimethyl-cyclohexane-1,2,3-trione-1,3-dioxime-2-phenylhydrazone (70820-93-8) → 4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one (97507-59-0)

Guidance literature:

With acetic anhydride; for 1h; Heating;

upstream raw materials:

(E)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime

(Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime

lead(IV) tetraacetate

5,5-dimethyl-1,3-bis(phenylhydrazono)-2-(p-tolylhydrazono)cyclohexane

Downstream raw materials:

4-(p-chlorophenylhydrazono)-6,6-dimethyl-2-phenyl-4,5,6,7-tetrahydro-2H-benzo-1,2,3-triazole

(E)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime p-toluenesulfonate

(Z)-4,5,6,7-tetrahydro-6,6-dimethyl-2-phenyl-2H-benzo<1,2,3>triazol-4-one oxime p-toluenesulfonate

5-acetyl-5,6,7,8-tetrahydro-7,7-dimethyl-2-phenyl-1,2,3-triazol<4,5-c>azepin-4-one

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