2-(3-{2-[2-(2H-Tetrazol-5-yl)-benzyl]-2H-tetrazol-5-yl}-phenoxymethyl)-quinoline

Base Information

Chemical Name:2-(3-{2-[2-(2H-Tetrazol-5-yl)-benzyl]-2H-tetrazol-5-yl}-phenoxymethyl)-quinoline
CAS No.:138786-30-8
Molecular Formula:C₂₅H₁₉N₉O
Molecular Weight:461.486
Hs Code.:

Synonyms:2-(3-{2-[2-(2H-Tetrazol-5-yl)-benzyl]-2H-tetrazol-5-yl}-phenoxymethyl)-quinoline

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Chemical Property of 2-(3-{2-[2-(2H-Tetrazol-5-yl)-benzyl]-2H-tetrazol-5-yl}-phenoxymethyl)-quinoline

Chemical Property:

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Technology Process of 2-(3-{2-[2-(2H-Tetrazol-5-yl)-benzyl]-2H-tetrazol-5-yl}-phenoxymethyl)-quinoline

There total 5 articles about 2-(3-{2-[2-(2H-Tetrazol-5-yl)-benzyl]-2H-tetrazol-5-yl}-phenoxymethyl)-quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 138786-32-0
2-<<5-<3-(quinolin-2-ylmethoxy)phenyl>-2H-tetrazol-2-yl>methyl>benzonitrile

: 138786-30-8
2-(3-{2-[2-(2H-Tetrazol-5-yl)-benzyl]-2H-tetrazol-5-yl}-phenoxymethyl)-quinoline

Guidance literature:: With lithium azide; triethylamine hydrobromide; In 2-methoxy-ethanol; at 120 ℃; for 3h;
DOI:10.1021/jm00085a005

Reference yield:

: 4377-41-7
2-Chloromethylquinoline

: 138786-30-8
2-(3-{2-[2-(2H-Tetrazol-5-yl)-benzyl]-2H-tetrazol-5-yl}-phenoxymethyl)-quinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, 0.5 h, 2.) DMF, 3 h

2: LiN₃, triethylammonium bromide / 2-methoxy-ethanol / 3 h / 120 °C

3: 74 percent / K₂CO₃, KI / butan-2-one / 8 h / Heating

4: LiN₃, triethylammonium bromide / 2-methoxy-ethanol / 3 h / 120 °C

With lithium azide; triethylamine hydrobromide; sodium hydride; potassium carbonate; potassium iodide; In 2-methoxy-ethanol; butanone;
DOI:10.1021/jm00085a005

Reference yield:

: 873-62-1
m-cyanophenol

: 138786-30-8
2-(3-{2-[2-(2H-Tetrazol-5-yl)-benzyl]-2H-tetrazol-5-yl}-phenoxymethyl)-quinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, 0.5 h, 2.) DMF, 3 h

2: LiN₃, triethylammonium bromide / 2-methoxy-ethanol / 3 h / 120 °C

3: 74 percent / K₂CO₃, KI / butan-2-one / 8 h / Heating

4: LiN₃, triethylammonium bromide / 2-methoxy-ethanol / 3 h / 120 °C

With lithium azide; triethylamine hydrobromide; sodium hydride; potassium carbonate; potassium iodide; In 2-methoxy-ethanol; butanone;
DOI:10.1021/jm00085a005