Technology Process of 1,1'-(3E)-deca-1,3-diene-1,1-diyldibenzene
There total 3 articles about 1,1'-(3E)-deca-1,3-diene-1,1-diyldibenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trans-bromo(N-succinimidyl)-bis(triphenylphosphine)palladium(II); sodium carbonate; tricyclohexylphosphine tetrafluoroborate;
In
tetrahydrofuran; water;
at 60 ℃;
for 20h;
Inert atmosphere;
Sealed vessel;
DOI:10.1016/j.tetlet.2012.04.091
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dimethyl sulfoxide / 3 h / 60 °C / Inert atmosphere
2: trans-bromo(N-succinimidyl)-bis(triphenylphosphine)palladium(II); sodium carbonate; tricyclohexylphosphine tetrafluoroborate / tetrahydrofuran; water / 20 h / 60 °C / Inert atmosphere; Sealed vessel
With
trans-bromo(N-succinimidyl)-bis(triphenylphosphine)palladium(II); sodium carbonate; tricyclohexylphosphine tetrafluoroborate;
In
tetrahydrofuran; water; dimethyl sulfoxide;
2: Suzuki-Miyaura coupling;
DOI:10.1016/j.tetlet.2012.04.091
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 20 - 70 °C / Inert atmosphere; Cooling with ice; Microwave irradiation; Neat (no solvent)
2: dimethyl sulfoxide / 3 h / 60 °C / Inert atmosphere
3: trans-bromo(N-succinimidyl)-bis(triphenylphosphine)palladium(II); sodium carbonate; tricyclohexylphosphine tetrafluoroborate / tetrahydrofuran; water / 20 h / 60 °C / Inert atmosphere; Sealed vessel
With
trans-bromo(N-succinimidyl)-bis(triphenylphosphine)palladium(II); sodium carbonate; tricyclohexylphosphine tetrafluoroborate;
In
tetrahydrofuran; water; dimethyl sulfoxide;
3: Suzuki-Miyaura coupling;
DOI:10.1016/j.tetlet.2012.04.091
