(2E)-3-phenyl-2-propenyl [(4-methylphenyl)sulfonyl] carbamic acid ester

Base Information

Chemical Name:(2E)-3-phenyl-2-propenyl [(4-methylphenyl)sulfonyl] carbamic acid ester
CAS No.:855422-02-5
Molecular Formula:C₁₇H₁₇NO₄S
Molecular Weight:331.392
Hs Code.:

Synonyms:(2E)-3-phenyl-2-propenyl [(4-methylphenyl)sulfonyl] carbamic acid ester

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Chemical Property of (2E)-3-phenyl-2-propenyl [(4-methylphenyl)sulfonyl] carbamic acid ester

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Technology Process of (2E)-3-phenyl-2-propenyl [(4-methylphenyl)sulfonyl] carbamic acid ester

There total 5 articles about (2E)-3-phenyl-2-propenyl [(4-methylphenyl)sulfonyl] carbamic acid ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 4083-64-1
Tosyl isocyanate

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 855422-02-5
(2E)-3-phenyl-2-propenyl [(4-methylphenyl)sulfonyl] carbamic acid ester

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/d1ob00670c

Reference yield: 95.0%

: 4393-06-0
1-Phenyl-2-propen-1-ol

: 4083-64-1
Tosyl isocyanate

: 855422-02-5
(2E)-3-phenyl-2-propenyl [(4-methylphenyl)sulfonyl] carbamic acid ester

Guidance literature:: In toluene; at 90 ℃; for 6h; Inert atmosphere;
DOI:10.1021/acs.joc.8b01320

Reference yield: 8.0%

: 591-50-4
iodobenzene

: 18303-03-2
prop-2-en-1-yl (4-methylbenzene-1-sulfonyl)carbamate

: 5848-57-7,32121-04-3,5882-85-9
4-methyl-N-[(2E)-3-phenylprop-2-en-1-yl]benzene-1-sulfonamide

: 2-phenylallyl tosylcarbamate

: 855422-02-5
(2E)-3-phenyl-2-propenyl [(4-methylphenyl)sulfonyl] carbamic acid ester

Guidance literature:: With tributylphosphine; potassium carbonate; palladium diacetate; In N,N-dimethyl-formamide; at 80 ℃; for 3h; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(00)73132-7