C₂₄H₂₉NO₄

Base Information

Chemical Name:C₂₄H₂₉NO₄
CAS No.:1259067-13-4
Molecular Formula:C₂₄H₂₉NO₄
Molecular Weight:395.499
Hs Code.:

C<sub>24</sub>H<sub>29</sub>NO<sub>4</sub>

Synonyms:C₂₄H₂₉NO₄

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Chemical Property of C₂₄H₂₉NO₄

Chemical Property:

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Technology Process of C₂₄H₂₉NO₄

There total 10 articles about C₂₄H₂₉NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1259067-10-1
C₂₈H₃₅Cl₃N₂O₅

: 1259067-13-4
C₂₄H₂₉NO₄

Guidance literature:: With potassium hydroxide; In water; tert-butyl alcohol; at 70 ℃; for 72h; Inert atmosphere;
DOI:10.1021/ol1026602

Reference yield: 56.0%

: C₂₈H₃₅Cl₃N₂O₅

: 1259067-13-4
C₂₄H₂₉NO₄

Guidance literature:: With potassium hydroxide; In water; tert-butyl alcohol; at 70 ℃; for 72h; Inert atmosphere;
DOI:10.1002/ejoc.201200523

Reference yield:

: 1259066-64-2
C₁₈H₂₆O₅

: 1259067-13-4
C₂₄H₂₉NO₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

1.2: 2.5 h / 0 - 20 °C / Inert atmosphere

2.1: water; acetic acid / 21.5 h / 20 - 40 °C / Inert atmosphere

3.1: o-xylene / 123 h / 20 - 160 °C / Inert atmosphere; Molecular sieve; Sealed tube

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 3.5 h / 0 - 20 °C / Inert atmosphere

5.1: potassium carbonate / o-xylene / 1.5 h / 140 °C / Inert atmosphere

6.1: potassium hydroxide / water; tert-butyl alcohol / 72 h / 70 °C / Inert atmosphere

With water; sodium hydride; potassium carbonate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium hydroxide; In dichloromethane; o-xylene; water; N,N-dimethyl-formamide; tert-butyl alcohol; 3.1: Claisen rearrangement / 5.1: Overman rearrangement;
DOI:10.1021/ol1026602