C₁₆H₂₁BrO₅

Base Information

Chemical Name:C₁₆H₂₁BrO₅
CAS No.:1514823-93-8
Molecular Formula:C₁₆H₂₁BrO₅
Molecular Weight:373.244
Hs Code.:

C<sub>16</sub>H<sub>21</sub>BrO<sub>5</sub>

Synonyms:C₁₆H₂₁BrO₅

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Chemical Property of C₁₆H₂₁BrO₅

Chemical Property:

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Technology Process of C₁₆H₂₁BrO₅

There total 8 articles about C₁₆H₂₁BrO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 1514823-92-7
C₈H₁₃BrO₄

: 1514823-93-8
C₁₆H₂₁BrO₅

Guidance literature:: p-Anisaldehyde dimethyl acetal; C₈H₁₃BrO₄; With toluene-4-sulfonic acid; In dichloromethane; water; at 0 ℃; for 2h;

With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol403220t

Reference yield:

: 183674-17-1
(1R,2S,5S,6R)-3,6-dibromo-1,2-O-isopropylidenecyclohex-3-ene-1,2,5-triol

: 1514823-93-8
C₁₆H₂₁BrO₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol / 14 h / 18 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

2.2: 4 h / 18 °C

3.1: acetic acid; water / 14 h / 70 °C

4.1: toluene-4-sulfonic acid / dichloromethane; water / 2 h / 0 °C

4.2: 6 h / -78 °C / Inert atmosphere

With water; sodium hydride; toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; methanol; dichloromethane; water; mineral oil;
DOI:10.1021/ol403220t

Reference yield:

: 1514823-90-5
C₁₁H₁₇BrO₄

: 1514823-93-8
C₁₆H₂₁BrO₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid; water / 14 h / 70 °C

2.1: toluene-4-sulfonic acid / dichloromethane; water / 2 h / 0 °C

2.2: 6 h / -78 °C / Inert atmosphere

With water; toluene-4-sulfonic acid; acetic acid; In dichloromethane; water;
DOI:10.1021/ol403220t