1,3-bis[(2-ethoxy tetrahydro-2H-pyran)]-2-O-benzyl glycerol

Base Information

Chemical Name:1,3-bis[(2-ethoxy tetrahydro-2H-pyran)]-2-O-benzyl glycerol
CAS No.:680219-93-6
Molecular Formula:C₂₄H₃₈O₇
Molecular Weight:438.562
Hs Code.:

Synonyms:1,3-bis[(2-ethoxy tetrahydro-2H-pyran)]-2-O-benzyl glycerol

Suppliers and Price of 1,3-bis[(2-ethoxy tetrahydro-2H-pyran)]-2-O-benzyl glycerol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,3-bis[(2-ethoxy tetrahydro-2H-pyran)]-2-O-benzyl glycerol

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 1,3-bis[(2-ethoxy tetrahydro-2H-pyran)]-2-O-benzyl glycerol

There total 1 articles about 1,3-bis[(2-ethoxy tetrahydro-2H-pyran)]-2-O-benzyl glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 17739-45-6,59146-56-4
2-(2-bromoethoxy)tetrahydropyran

: 14690-00-7
2-O-benzylglycerol

: 680219-93-6
1,3-bis[(2-ethoxy tetrahydro-2H-pyran)]-2-O-benzyl glycerol

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 24h;
DOI:10.1016/j.tetlet.2004.02.044

Reference yield: 88.0%

: 680219-93-6
1,3-bis[(2-ethoxy tetrahydro-2H-pyran)]-2-O-benzyl glycerol

: 680219-94-7
3,7-dioxa-5-O-benzyl-1,9-nonanediol

Guidance literature:: With hydrogenchloride; methanol; In diethyl ether; at 20 ℃; for 2h;
DOI:10.1016/j.tetlet.2004.02.044

Reference yield:

: 680219-93-6
1,3-bis[(2-ethoxy tetrahydro-2H-pyran)]-2-O-benzyl glycerol

: 680219-95-8
1,9-dibromo-3,7-dioxa-5-O-benzyl-1,9-nonane

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / hydrochloric acid / diethyl ether; methanol / 2 h / 20 °C

2: 91 percent / triphenylphosphine; CBr₄ / CH₂Cl₂ / 2 h / 0 °C

With hydrogenchloride; carbon tetrabromide; triphenylphosphine; In methanol; diethyl ether; dichloromethane;
DOI:10.1016/j.bioorg.2005.06.001