N²,N²-(1,5-citryl)bis6-acetyl-N⁶-(benzyloxy)-(L)-lysine>

Base Information

Chemical Name:N²,N²-(1,5-citryl)bis6-acetyl-N⁶-(benzyloxy)-(L)-lysine>
CAS No.:81505-63-7
Molecular Formula:C₃₉H₅₄N₄O₁₃
Molecular Weight:786.877
Hs Code.:

N<sup>2</sup>,N<sup>2</sup>-(1,5-citryl)bis<N<sup>6</sup>-acetyl-N<sup>6</sup>-(benzyloxy)-(L)-lysine>

Synonyms:N²,N²-(1,5-citryl)bis6-acetyl-N⁶-(benzyloxy)-(L)-lysine>

Suppliers and Price of N²,N²-(1,5-citryl)bis6-acetyl-N⁶-(benzyloxy)-(L)-lysine>

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N²,N²-(1,5-citryl)bis6-acetyl-N⁶-(benzyloxy)-(L)-lysine>

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N²,N²-(1,5-citryl)bis6-acetyl-N⁶-(benzyloxy)-(L)-lysine>

There total 8 articles about N²,N²-(1,5-citryl)bis6-acetyl-N⁶-(benzyloxy)-(L)-lysine> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.5%

: 81505-62-6
N²,N²-(anhydromethylene-1,5-citryl)bis6-acetyl-N⁶-(benzyloxy)-(L)-lysine methyl ester

: 81505-63-7
N²,N²-(1,5-citryl)bis6-acetyl-N⁶-(benzyloxy)-(L)-lysine>

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; for 2h; Ambient temperature;
DOI:10.1021/ja00375a025

Reference yield:

: 5462-80-6
rac-6-hydroxynorleucine

: 81505-63-7
N²,N²-(1,5-citryl)bis6-acetyl-N⁶-(benzyloxy)-(L)-lysine>

Guidance literature:: Multi-step reaction with 7 steps

1: Et₃N / tetrahydrofuran; H₂O / Ambient temperature

2: CH₂Cl₂ / 20 h / Heating

3: CBr₄, PPh₃ / tetrahydrofuran / Ambient temperature

4: KI, K₂CO₃ / acetone / Heating

5: CF₃CO₂H / 0.08 h / Ambient temperature

6: CHCl₃ / 1.) 0 deg C, 5 min, 2.) room temperature, 40 min

7: 98.5 percent / NaOH / tetrahydrofuran; H₂O / 2 h / Ambient temperature

With sodium hydroxide; carbon tetrabromide; potassium carbonate; triethylamine; triphenylphosphine; trifluoroacetic acid; potassium iodide; In tetrahydrofuran; dichloromethane; chloroform; water; acetone;
DOI:10.1021/ja00375a025

Reference yield:

: 81505-61-5
(4-Oxo-1,3-dioxolan-5-ylidene)diacetyl chloride

: 81505-63-7
N²,N²-(1,5-citryl)bis6-acetyl-N⁶-(benzyloxy)-(L)-lysine>

Guidance literature:: Multi-step reaction with 2 steps

1: CHCl₃ / 1.) 0 deg C, 5 min, 2.) room temperature, 40 min

2: 98.5 percent / NaOH / tetrahydrofuran; H₂O / 2 h / Ambient temperature

With sodium hydroxide; In tetrahydrofuran; chloroform; water;
DOI:10.1021/ja00375a025