N-(5,5-dimethylhexa-2,3-dien-1-yl)-4-methyl-N-(7-oxohept-2-yn-1-yl)benzenesulfonamide

Base Information

Chemical Name:N-(5,5-dimethylhexa-2,3-dien-1-yl)-4-methyl-N-(7-oxohept-2-yn-1-yl)benzenesulfonamide
CAS No.:1449486-48-9
Molecular Formula:C₂₂H₂₉NO₃S
Molecular Weight:387.543
Hs Code.:

Synonyms:N-(5,5-dimethylhexa-2,3-dien-1-yl)-4-methyl-N-(7-oxohept-2-yn-1-yl)benzenesulfonamide

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Chemical Property of N-(5,5-dimethylhexa-2,3-dien-1-yl)-4-methyl-N-(7-oxohept-2-yn-1-yl)benzenesulfonamide

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Technology Process of N-(5,5-dimethylhexa-2,3-dien-1-yl)-4-methyl-N-(7-oxohept-2-yn-1-yl)benzenesulfonamide

There total 4 articles about N-(5,5-dimethylhexa-2,3-dien-1-yl)-4-methyl-N-(7-oxohept-2-yn-1-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₉NO₃S

: 1449486-48-9
N-(5,5-dimethylhexa-2,3-dien-1-yl)-4-methyl-N-(7-oxohept-2-yn-1-yl)benzenesulfonamide

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1016/j.tet.2013.04.068

Reference yield:

: 121352-64-5
(Z)-7-((tert-butyldimethylsilyl)oxy)hept-2-yne-1-ol

: 1449486-48-9
N-(5,5-dimethylhexa-2,3-dien-1-yl)-4-methyl-N-(7-oxohept-2-yn-1-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 42 h / 0 - 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 21 h / 0 - 20 °C / Inert atmosphere

3: Dess-Martin periodane / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; Dess-Martin periodane; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2013.04.068

Reference yield:

: C₁₄H₁₉NO₂S

: 1449486-48-9
N-(5,5-dimethylhexa-2,3-dien-1-yl)-4-methyl-N-(7-oxohept-2-yn-1-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 42 h / 0 - 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 21 h / 0 - 20 °C / Inert atmosphere

3: Dess-Martin periodane / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; Dess-Martin periodane; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2013.04.068