3-[3-Oxo-3-piperidin-1-yl-2-(toluene-4-sulfonylamino)-propyl]-benzamidine; hydriodide

Base Information

Chemical Name:3-[3-Oxo-3-piperidin-1-yl-2-(toluene-4-sulfonylamino)-propyl]-benzamidine; hydriodide
CAS No.:71078-73-4
Molecular Formula:C₂₂H₂₈N₄O₃S*HI
Molecular Weight:556.468
Hs Code.:

Synonyms:3-[3-Oxo-3-piperidin-1-yl-2-(toluene-4-sulfonylamino)-propyl]-benzamidine; hydriodide

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Chemical Property of 3-[3-Oxo-3-piperidin-1-yl-2-(toluene-4-sulfonylamino)-propyl]-benzamidine; hydriodide

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Technology Process of 3-[3-Oxo-3-piperidin-1-yl-2-(toluene-4-sulfonylamino)-propyl]-benzamidine; hydriodide

There total 9 articles about 3-[3-Oxo-3-piperidin-1-yl-2-(toluene-4-sulfonylamino)-propyl]-benzamidine; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 80853-27-6
3-[3-Oxo-3-piperidin-1-yl-2-(toluene-4-sulfonylamino)-propyl]-thiobenzimidic acid methyl ester; hydriodide

: 71078-73-4
3-[3-Oxo-3-piperidin-1-yl-2-(toluene-4-sulfonylamino)-propyl]-benzamidine; hydriodide

Guidance literature:: With ammonium acetate; In ethanol; at 70 - 80 ℃; for 2.5h;

Reference yield:

: 52117-00-7
2-Acetylamino-2-[(3-cyanophenyl)-methyl]-malonic acid diethyl ester

: 71078-73-4
3-[3-Oxo-3-piperidin-1-yl-2-(toluene-4-sulfonylamino)-propyl]-benzamidine; hydriodide

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) 3 M HCl, 2.) 1 M KOH / 1.) acetic acid, 6 h, reflux, 2.) ether, 12 h, r.t.

2: SOCl₂ / 1 h / Heating

3: 42 percent / benzene / 1.5 h / Ambient temperature

4: 97 percent / H₂S(gas), TEA / pyridine / 72 h / Ambient temperature

5: 70 percent / acetone / 27 h / Ambient temperature

6: 72 percent / Ammonium acetate / ethanol / 2.5 h / 70 - 80 °C

With ammonium acetate; hydrogenchloride; potassium hydroxide; thionyl chloride; TEA; hydrogen sulfide; In pyridine; ethanol; acetone; benzene;

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 71078-73-4
3-[3-Oxo-3-piperidin-1-yl-2-(toluene-4-sulfonylamino)-propyl]-benzamidine; hydriodide

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) 3 M HCl, 2.) 1 M KOH / 1.) acetic acid, 6 h, reflux, 2.) ether, 12 h, r.t.

2: SOCl₂ / 1 h / Heating

3: 42 percent / benzene / 1.5 h / Ambient temperature

4: 97 percent / H₂S(gas), TEA / pyridine / 72 h / Ambient temperature

5: 70 percent / acetone / 27 h / Ambient temperature

6: 72 percent / Ammonium acetate / ethanol / 2.5 h / 70 - 80 °C

With ammonium acetate; hydrogenchloride; potassium hydroxide; thionyl chloride; TEA; hydrogen sulfide; In pyridine; ethanol; acetone; benzene;