Technology Process of C16H13BrO4S
There total 3 articles about C16H13BrO4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
for 1h;
Heating;
DOI:10.1080/00397910701471246
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 88 percent / benzyltriethylammonium chloride; aq. NaOH / CH2Cl2 / 0.5 h / 20 °C
2: 92 percent / m-CPBA / CH2Cl2 / 1 h / Heating
With
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
DOI:10.1080/00397910701471246
- Guidance literature:
-
Multi-step reaction with 3 steps
1: phosphorous pentasulfide; sodium bicarbonate / tetrahydrofuran / 2 h / 20 °C
2: 88 percent / benzyltriethylammonium chloride; aq. NaOH / CH2Cl2 / 0.5 h / 20 °C
3: 92 percent / m-CPBA / CH2Cl2 / 1 h / Heating
With
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; phosphorous (V) sulfide; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1080/00397910701471246