7-(2-chlorophenyl)-7-(6,7-dihydro-4H-thieno[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

Base Information

Chemical Name:7-(2-chlorophenyl)-7-(6,7-dihydro-4H-thieno[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride
CAS No.:1373491-53-2
Molecular Formula:C₂₂H₂₈ClNO₂S*ClH
Molecular Weight:442.45
Hs Code.:

Synonyms:7-(2-chlorophenyl)-7-(6,7-dihydro-4H-thieno[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

Suppliers and Price of 7-(2-chlorophenyl)-7-(6,7-dihydro-4H-thieno[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-(2-chlorophenyl)-7-(6,7-dihydro-4H-thieno[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-(2-chlorophenyl)-7-(6,7-dihydro-4H-thieno[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

There total 5 articles about 7-(2-chlorophenyl)-7-(6,7-dihydro-4H-thieno[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1373491-74-7
7-(2-chlorophenyl)-7-(6,7-dihydro-4H-thieno[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid ethyl ester

: 1373491-53-2
7-(2-chlorophenyl)-7-(6,7-dihydro-4H-thieno[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

Guidance literature:: 7-(2-chlorophenyl)-7-(6,7-dihydro-4H-thieno[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid ethyl ester; With water; potassium hydroxide; In ethanol; for 24h; Reflux;

With hydrogenchloride; In water;

Reference yield:

: 1373492-24-0
(5-ethoxycarbonyl-5-methylhexyl)-triphenylphosphonium bromide

: 1373491-53-2
7-(2-chlorophenyl)-7-(6,7-dihydro-4H-thieno[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / dichloromethane; water / 2.17 h / 20 °C

2: hydrogen bromide; acetic acid / 3 h / 20 °C / Inert atmosphere; Cooling in ice-water bath

3: potassium carbonate / N,N-dimethyl-formamide / 44 h / 75 °C / Inert atmosphere

4: potassium hydroxide; water / ethanol / 24 h / Reflux

With water; hydrogen bromide; potassium carbonate; acetic acid; potassium hydroxide; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1373492-27-3
7-bromo-7-(2-chlorophenyl)-2,2-dimethylheptanoic acid ethyl ester

: 1373491-53-2
7-(2-chlorophenyl)-7-(6,7-dihydro-4H-thieno[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 44 h / 75 °C / Inert atmosphere

2: potassium hydroxide; water / ethanol / 24 h / Reflux

With water; potassium carbonate; potassium hydroxide; In ethanol; N,N-dimethyl-formamide;