benzyl-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1-4)-O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-benzyl-β-D-glucopyranosid

Base Information

Chemical Name:benzyl-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1-4)-O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-benzyl-β-D-glucopyranosid
CAS No.:97604-28-9
Molecular Formula:C₇₄H₇₇NO₂₀
Molecular Weight:1300.42
Hs Code.:

benzyl-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1-4)-O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-benzyl-β-D-glucopyranosid

Synonyms:benzyl-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1-4)-O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-benzyl-β-D-glucopyranosid

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Chemical Property of benzyl-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1-4)-O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-benzyl-β-D-glucopyranosid

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Technology Process of benzyl-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1-4)-O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-benzyl-β-D-glucopyranosid

There total 1 articles about benzyl-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1-4)-O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-benzyl-β-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.5%

: 94926-36-0
benzyl 2,3,6-tri-O-benzyl-4-O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

: 110455-06-6
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-α,β-D-galactopyranosyl bromide

: 97604-28-9
benzyl-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1-4)-O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-benzyl-β-D-glucopyranosid

: 97604-27-8
benzyl-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1-3)-O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-benzyl-β-D-glucopyranosid

Guidance literature:: With mercury(II) cyanide; mercury dibromide; In nitromethane; toluene; at 20 ℃; for 5h; Product distribution; various catalysts; investigation of the regiochemistry of the coupling reactions;
DOI:10.1016/0008-6215(85)85148-X

Reference yield: 95.0%

: 108-24-7
acetic anhydride

: 97604-28-9
benzyl-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1-4)-O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-benzyl-β-D-glucopyranosid

: 97626-41-0
benzyl-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1-4)-O-(3-O-acetyl-2,6-di-O-benzyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-benzyl-β-D-glucopyranosid

Guidance literature:: In pyridine; at 20 ℃; for 24h;
DOI:10.1016/0008-6215(85)85148-X

Reference yield:

: 108-24-7
acetic anhydride

: 97604-28-9
benzyl-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-galactopyranosyl)-(1-4)-O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-benzyl-β-D-glucopyranosid

: 97604-32-5
benzyl-O-(2-acetamido-2-desoxy-β-D-galactopyranosyl)-(1-4)-O-(2,6-di-O-benzyl-β-D-galactopyranosyl)-(1-4)-2,3,6-tri-O-benzyl-β-D-glucopyranosid

Guidance literature:: With N-butylamine; Yield given. Multistep reaction; 1.) methanol, reflux, 4 h; 1.) methanol, 0 deg C, 3 h;
DOI:10.1016/0008-6215(85)85148-X