2-(2-Nitroaethyl)-4-nitrophenol

Base Information

• Chemical Name: 2-(2-Nitroaethyl)-4-nitrophenol
• CAS No.: 69957-38-6
• Molecular Formula: C₈H₈N₂O₅
• Molecular Weight: 212.162
• Mol file: 69957-38-6.mol

Synonyms:2-(2-Nitroaethyl)-4-nitrophenol

Chemical Property of 2-(2-Nitroaethyl)-4-nitrophenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 2-(2-Nitroaethyl)-4-nitrophenol

There total 3 articles about 2-(2-Nitroaethyl)-4-nitrophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C8H6N2O5 → 2-(2-Nitroaethyl)-4-nitrophenol (69957-38-6)

Guidance literature:

With methanol; sodium tetrahydroborate; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.chempr.2017.06.015

Reference yield:

5-Nitrosalicylaldehyde (97-51-8) → 2-(2-Nitroaethyl)-4-nitrophenol (69957-38-6)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium acetate / 100 °C / Inert atmosphere

2: sodium tetrahydroborate; methanol / 0 - 20 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; ammonium acetate;

DOI:10.1016/j.chempr.2017.06.015

Reference yield:

3,6-dinitro-coumarin (37630-80-1) → 2-(2-Nitroaethyl)-4-nitrophenol (69957-38-6)

Guidance literature:

With formic acid; triethylamine; In N,N-dimethyl-formamide;

upstream raw materials:

3,6-dinitro-coumarin

5-Nitrosalicylaldehyde

Downstream raw materials:

2,5-dinitrobenzofuran