N,N'-bis(2,6-bis(3,5-dimethylphenyl)phenyl)-1,4-diaza-2,3-dimethyl-butadiene

Base Information

Chemical Name:N,N'-bis(2,6-bis(3,5-dimethylphenyl)phenyl)-1,4-diaza-2,3-dimethyl-butadiene
CAS No.:340187-62-4
Molecular Formula:C₄₈H₄₈N₂
Molecular Weight:652.923
Hs Code.:

Synonyms:N,N'-bis(2,6-bis(3,5-dimethylphenyl)phenyl)-1,4-diaza-2,3-dimethyl-butadiene

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Chemical Property of N,N'-bis(2,6-bis(3,5-dimethylphenyl)phenyl)-1,4-diaza-2,3-dimethyl-butadiene

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Technology Process of N,N'-bis(2,6-bis(3,5-dimethylphenyl)phenyl)-1,4-diaza-2,3-dimethyl-butadiene

There total 3 articles about N,N'-bis(2,6-bis(3,5-dimethylphenyl)phenyl)-1,4-diaza-2,3-dimethyl-butadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 431-03-8
dimethylglyoxal

: 340187-65-7
3,5,3'',5''-tetramethyl-1,1':3',1''-terphenyl-2'-ylamine

: 340187-62-4
N,N'-bis(2,6-bis(3,5-dimethylphenyl)phenyl)-1,4-diaza-2,3-dimethyl-butadiene

Guidance literature:: toluene-4-sulfonic acid; In benzene; for 40h; Heating;
DOI:10.1021/ja070224i

Reference yield:

: 608-30-0
2,6-dibromoaniline

: 340187-62-4
N,N'-bis(2,6-bis(3,5-dimethylphenyl)phenyl)-1,4-diaza-2,3-dimethyl-butadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / aq. Na₂CO₃ / Pd(PPh₃)4 / benzene; ethanol / 48 h / Heating

2: 56 percent / p-toluenesulfonic acid monohydrate / benzene / 40 h / Heating

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; toluene-4-sulfonic acid; In ethanol; benzene; 1: Suzuki reaction;
DOI:10.1021/ja070224i

Reference yield:

: 172975-69-8
3,5-dimethylphenyl boronic acid

: 340187-62-4
N,N'-bis(2,6-bis(3,5-dimethylphenyl)phenyl)-1,4-diaza-2,3-dimethyl-butadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / aq. Na₂CO₃ / Pd(PPh₃)4 / benzene; ethanol / 48 h / Heating

2: 56 percent / p-toluenesulfonic acid monohydrate / benzene / 40 h / Heating

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; toluene-4-sulfonic acid; In ethanol; benzene; 1: Suzuki reaction;
DOI:10.1021/ja070224i