(S)-2-(1,2-diphenylpropan-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(S)-2-(1,2-diphenylpropan-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1201898-81-8
Molecular Formula:C₂₁H₂₇BO₂
Molecular Weight:322.255
Hs Code.:

Synonyms:(S)-2-(1,2-diphenylpropan-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of (S)-2-(1,2-diphenylpropan-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of (S)-2-(1,2-diphenylpropan-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 1 articles about (S)-2-(1,2-diphenylpropan-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 133038-74-1
(S)-(-)-1-phenylethyl N,N-diisopropylcarbamate

: 87100-28-5
pinacol benzylboronate

: 1201898-81-8
(S)-2-(1,2-diphenylpropan-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: (S)-(-)-1-phenylethyl N,N-diisopropylcarbamate; With sec.-butyllithium; In diethyl ether; hexane; cyclohexane; at -75 - -70 ℃; Inert atmosphere;

pinacol benzylboronate; In diethyl ether; hexane; cyclohexane; at -70 - 25 ℃; for 4.75h; Inert atmosphere;
DOI:10.1016/j.tet.2009.10.002

Reference yield: 99.0%

: 1201898-81-8
(S)-2-(1,2-diphenylpropan-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: potassium (S)-(1,2-diphenylprop-2-yl)trifluoroborate

Guidance literature:: With potassium hydrogenfluoride; water; In methanol; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.10.002

Reference yield: 84.0%

: 1201898-81-8
(S)-2-(1,2-diphenylpropan-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 5814-85-7
1,2-diphenylpropane

Guidance literature:: With O-Methylhydroxylamin; potassium tert-butylate; In tetrahydrofuran; toluene; at 80 ℃; for 16h; Inert atmosphere; Sealed tube;
DOI:10.1055/s-0037-1610172