[1-(5-hydroxy-3-methyl-4,5-dihydro-isoxazol-5-yl)-2-azabicyclo[2.1.1]hex-2-yl]phenylmethanone

Base Information

Chemical Name:[1-(5-hydroxy-3-methyl-4,5-dihydro-isoxazol-5-yl)-2-azabicyclo[2.1.1]hex-2-yl]phenylmethanone
CAS No.:1072914-13-6
Molecular Formula:C₁₆H₁₈N₂O₃
Molecular Weight:286.331
Hs Code.:

Synonyms:[1-(5-hydroxy-3-methyl-4,5-dihydro-isoxazol-5-yl)-2-azabicyclo[2.1.1]hex-2-yl]phenylmethanone

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Chemical Property of [1-(5-hydroxy-3-methyl-4,5-dihydro-isoxazol-5-yl)-2-azabicyclo[2.1.1]hex-2-yl]phenylmethanone

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Technology Process of [1-(5-hydroxy-3-methyl-4,5-dihydro-isoxazol-5-yl)-2-azabicyclo[2.1.1]hex-2-yl]phenylmethanone

There total 1 articles about [1-(5-hydroxy-3-methyl-4,5-dihydro-isoxazol-5-yl)-2-azabicyclo[2.1.1]hex-2-yl]phenylmethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 127-06-0
acetone oxime

: 637739-93-6
2-benzoyl-2-azabicyclo[2.1.1]hexane-1-carboxylic acid ethyl ester

: 1072914-13-6
[1-(5-hydroxy-3-methyl-4,5-dihydro-isoxazol-5-yl)-2-azabicyclo[2.1.1]hex-2-yl]phenylmethanone

Guidance literature:: acetone oxime; With tert.-butyl lithium; In tetrahydrofuran; hexane; at 0 ℃; for 2h; Inert atmosphere;

2-benzoyl-2-azabicyclo[2.1.1]hexane-1-carboxylic acid ethyl ester; In tetrahydrofuran; hexane; at 0 ℃; for 20h; Inert atmosphere;
DOI:10.1021/jm800537a